Catalytic thiomethylation of N-substituted ureas and thioureas with N,N,N',N'-tetramethylmethanediamine and α,ω-alkanedithiols

被引：2

作者：

Khairullina, R. R. ^{[1
]}

Geniyatova, A. R. ^{[1
]}

Meshcheryakova, E. S. ^{[1
]}

Tyumkina, T. V. ^{[1
]}

Khalilov, L. M. ^{[1
]}

Ibragimov, A. G. ^{[1
]}

Dzhemilev, U. M. ^{[1
]}

机构：

[1] Russian Acad Sci, Inst Petrochem & Catalysis, Pr Oktyabrya 141, Ufa 450075, Bashkortostan, Russia

来源：

RUSSIAN JOURNAL OF ORGANIC CHEMISTRY | 2017年 / 53卷 / 03期

基金：

俄罗斯基础研究基金会;

关键词：

CARBOXYLIC-ACID HYDRAZIDES; ANTIMICROBIAL ACTIVITY; N,6-DIARYL-4-METHYL-2-THIOXO-1,2,3,6-TETRAHYDROPYRIMIDINE-5-CARBOXAMIDES; H2S;

D O I：

10.1134/S1070428017030010

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

An efficient procedure has been developed for the synthesis of N,N'-(2,5-dithiaalkane-alpha,omega-diyl)bis-(N'-allylthioureas) by thiomethylation of N-substituted ureas and thioureas with alpha,omega-alkanedithiols and N,N,N',N'-tetramethylmethanediamine in the presence of cesium carbonate as catalyst.

引用

页码：315 / 321

页数：7

共 50 条

[1] Catalytic thiomethylation of N-substituted ureas and thioureas with N,N,N′,N′-tetramethylmethanediamine and α,ω-alkanedithiols
R. R. Khairullina
A. R. Geniyatova
E. S. Meshcheryakova
T. V. Tyumkina
L. M. Khalilov
A. G. Ibragimov
U. M. Dzhemilev
Russian Journal of Organic Chemistry, 2017, 53 : 315 - 321
[2] THE REACTION OF ENONES WITH N-SUBSTITUTED HYDRAZINES AND N-SUBSTITUTED UREAS
KASHIMA, C
YOSHIWARA, N
HETEROCYCLES, 1985, 23 (01) : 171 - 171
[3] Bismuth(III) complexing with some N- and N,N-substituted thioureas
N. N. Golovnev
G. V. Novikova
A. A. Leshok
Russian Journal of Inorganic Chemistry, 2009, 54 : 329 - 331
[4] Bismuth(III) Complexing with Some N- and N,N-Substituted Thioureas
Golovnev, N. N.
Novikova, G. V.
Leshok, A. A.
RUSSIAN JOURNAL OF INORGANIC CHEMISTRY, 2009, 54 (02) : 329 - 331
[5] Catalytic thiomethylation of regioisomeric aminobenzamides using bis(N,N-dimethylamino)methane and α,ω-alkanedithiols
R. R. Khairullina
T. V. Tyumkina
A. G. Ibragimov
Russian Chemical Bulletin, 2021, 70 : 757 - 762
[6] Catalytic thiomethylation of regioisomeric aminobenzamides using bis(N,N-dimethylamino)methane and α,ω-alkanedithiols
Khairullina, R. R.
Tyumkina, T., V
Ibragimov, A. G.
RUSSIAN CHEMICAL BULLETIN, 2021, 70 (04) : 757 - 762
[7] THE SYNTHESIS OF N-SUBSTITUTED UREAS .1. THE N-ALKYLATION OF UREAS
HACKL, KA
FALK, H
MONATSHEFTE FUR CHEMIE, 1992, 123 (6-7): : 599 - 606
[8] THE CONDENSATION OF N-SUBSTITUTED MALEIMIDES WITH THIOUREAS
MARRIAN, DH
JOURNAL OF THE CHEMICAL SOCIETY, 1949, (JUL): : 1797 - 1799
[9] Catalytic cycloaminomethylation of ureas and thioureas with N,N-bis(methoxymethyl)alkanamines
Khairullina, R. R.
Geniyatova, A. R.
Meshcheryakova, E. S.
Khalilov, L. M.
Ibragimov, A. G.
Dzhemilev, U. M.
RUSSIAN JOURNAL OF ORGANIC CHEMISTRY, 2015, 51 (01) : 116 - 120
[10] Catalytic cycloaminomethylation of ureas and thioureas with N,N-bis(methoxymethyl)alkanamines
R. R. Khairullina
A. R. Geniyatova
E. S. Meshcheryakova
L. M. Khalilov
A. G. Ibragimov
U. M. Dzhemilev
Russian Journal of Organic Chemistry, 2015, 51 : 116 - 120

← 1 2 3 4 5 →