Catalytic thiomethylation of N-substituted ureas and thioureas with N,N,N',N'-tetramethylmethanediamine and α,ω-alkanedithiols

被引：2

作者：

Khairullina, R. R. ^{[1
]}

Geniyatova, A. R. ^{[1
]}

Meshcheryakova, E. S. ^{[1
]}

Tyumkina, T. V. ^{[1
]}

Khalilov, L. M. ^{[1
]}

Ibragimov, A. G. ^{[1
]}

Dzhemilev, U. M. ^{[1
]}

机构：

[1] Russian Acad Sci, Inst Petrochem & Catalysis, Pr Oktyabrya 141, Ufa 450075, Bashkortostan, Russia

来源：

RUSSIAN JOURNAL OF ORGANIC CHEMISTRY | 2017年 / 53卷 / 03期

基金：

俄罗斯基础研究基金会;

关键词：

CARBOXYLIC-ACID HYDRAZIDES; ANTIMICROBIAL ACTIVITY; N,6-DIARYL-4-METHYL-2-THIOXO-1,2,3,6-TETRAHYDROPYRIMIDINE-5-CARBOXAMIDES; H2S;

D O I：

10.1134/S1070428017030010

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

An efficient procedure has been developed for the synthesis of N,N'-(2,5-dithiaalkane-alpha,omega-diyl)bis-(N'-allylthioureas) by thiomethylation of N-substituted ureas and thioureas with alpha,omega-alkanedithiols and N,N,N',N'-tetramethylmethanediamine in the presence of cesium carbonate as catalyst.

引用

页码：315 / 321

页数：7

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