Catalytic cycloaminomethylation of ureas and thioureas with N,N-bis(methoxymethyl)alkanamines

被引：0
|
作者：
R. R. Khairullina
A. R. Geniyatova
E. S. Meshcheryakova
L. M. Khalilov
A. G. Ibragimov
U. M. Dzhemilev
机构：
[1] Russian Academy of Sciences,Institute of Petrochemistry and Catalysis
来源：
Russian Journal of Organic Chemistry | 2015年 / 51卷
关键词：
Dione; Thiourea; Colorless Crystal; Triazinane Ring; Methoxymethyl;
D O I：
暂无
中图分类号：
学科分类号：
摘要：
An efficient procedure has been developed for the synthesis of 5-alkyl-1,3,5-triazinan-2-ones, 5-alkyl-1,3,5-triazinane-2-thiones, and 2,6-dialkylhexahydro-2,3a,4a,6,7a,8a-hexaazacyclopenta[def]fluorene-4,8(1H,5H)-diones by reactions of urea, thiourea, and tetrahydroimidazo[4,5-d]imidazole-2,5-(1H,3H)-dione with N,N-bis(methoxymethyl)alkanamines in the presence of SmCl3 · 6 H2O as catalyst.
引用
收藏
页码：116 / 120
页数：4
相关论文
共 50 条
  • [1] Catalytic cycloaminomethylation of ureas and thioureas with N,N-bis(methoxymethyl)alkanamines
    Khairullina, R. R.
    Geniyatova, A. R.
    Meshcheryakova, E. S.
    Khalilov, L. M.
    Ibragimov, A. G.
    Dzhemilev, U. M.
    [J]. RUSSIAN JOURNAL OF ORGANIC CHEMISTRY, 2015, 51 (01) : 116 - 120
  • [2] Catalytic thiomethylation of N-substituted ureas and thioureas with N,N,N',N'-tetramethylmethanediamine and α,ω-alkanedithiols
    Khairullina, R. R.
    Geniyatova, A. R.
    Meshcheryakova, E. S.
    Tyumkina, T. V.
    Khalilov, L. M.
    Ibragimov, A. G.
    Dzhemilev, U. M.
    [J]. RUSSIAN JOURNAL OF ORGANIC CHEMISTRY, 2017, 53 (03) : 315 - 321
  • [3] Catalytic thiomethylation of N-substituted ureas and thioureas with N,N,N′,N′-tetramethylmethanediamine and α,ω-alkanedithiols
    R. R. Khairullina
    A. R. Geniyatova
    E. S. Meshcheryakova
    T. V. Tyumkina
    L. M. Khalilov
    A. G. Ibragimov
    U. M. Dzhemilev
    [J]. Russian Journal of Organic Chemistry, 2017, 53 : 315 - 321
  • [4] Synthesis and anticancer activity of N-bis(trifluoromethyl)alkyl-N′-thiazolyl and N-bis(trifluoromethyl)alkyl-N′-benzothiazolyl ureas
    Luzina, Elena L.
    Popov, Anatoliy V.
    [J]. EUROPEAN JOURNAL OF MEDICINAL CHEMISTRY, 2009, 44 (12) : 4944 - 4953
  • [5] Intramolecular conversion of N,N-bis(2-picolyl)ureas to cyclic carbamates
    Jakob, Uwe
    Bannwarth, Willi
    [J]. TETRAHEDRON LETTERS, 2015, 56 (46) : 6340 - 6344
  • [6] ALPHA-HYDROXYCARBOXAMIDES FROM N,N-BIS(METHOXYMETHYL)CARBAMOYLLITHIUM AND CARBONYL-COMPOUNDS
    SCHOLLKOPF, U
    BECKHAUS, H
    [J]. ANGEWANDTE CHEMIE-INTERNATIONAL EDITION IN ENGLISH, 1976, 15 (05): : 293 - 293
  • [7] SYNTHESIS OF N,N-BIS(ARYL)-N-(2-THIAZOLIN-2-YL)THIOUREAS
    GONZALEZ, MA
    CABALLERO, RB
    MORENO, PC
    REQUEJO, JLJ
    ALBARRAN, JCP
    [J]. HETEROCYCLES, 1990, 30 (01) : 463 - 469
  • [8] PREPARATION AND PROPERTIES OF SURFACTANTS OF THE TYPE OF DISODIUM SALTS OF N,N-BIS(2-SULFOETHYL)-1-ALKANAMINES.
    Tomson, R.
    Faingol'd, S.I.
    [J]. Journal of applied chemistry of the USSR, 1984, 57 (9 pt 2): : 1885 - 1891
  • [9] PREPARATION AND PROPERTIES OF SURFACTANTS OF THE TYPE OF DISODIUM SALTS OF "N,N-BIS(2-SULFOETHYL)-1-ALKANAMINES
    TOMSON, R
    FAINGOLD, SI
    [J]. JOURNAL OF APPLIED CHEMISTRY OF THE USSR, 1984, 57 (09): : 1885 - 1891
  • [10] USE OF NUCLEAR MAGNETIC RESONANCE IN STUDIES OF TEXTILE FINISHING AGENTS . N,N-BIS (METHOXYMETHYL) AMIDES AND N,N-DIMETHYLOLAMIDES
    VAIL, SL
    SNOWDEN, FW
    MCCALL, ER
    [J]. AMERICAN DYESTUFF REPORTER, 1967, 56 (22): : 60 - &
12345