Three-component one-pot reaction for the synthesis of β-amide ketones

被引：3

作者：

Luo, Yan-Ping ^{[1
]}

Chen, Qiong ^{[2
]}

机构：

[1] Hainan Univ, Key Lab Protect & Dev Utilisat Trop Crop Germplas, Minist Educ, Haikou 570228, Peoples R China

[2] Cent China Normal Univ, Key Lab Pesticide & Chem Biol, Minist Educ, Coll Chem, Wuhan 430079, Peoples R China

来源：

CHEMICAL PAPERS | 2013年 / 67卷 / 05期

基金：

中国国家自然科学基金;

关键词：

beta-amide ketones; one-pot reaction; synthesis; DAKIN-WEST REACTION; ACETAMIDO KETONES; EFFICIENT; CATALYST; PROPARGYLAMINES; ALDEHYDES; ALKYNES; ACIDS;

D O I：

10.2478/s11696-013-0313-0

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

beta-amide ketones were synthesised by a three-component one-pot reaction of phenylacetylene, aldehydes, and amides in anhydrous acetonitrile containing trifluoroacetic acid and acetic acid in the presence of AlCl3 catalyst. The title compound structures were identified by H-1 NMR, C-13 NMR, MS, and elemental analysis.

引用

下载

页码：532 / 537

页数：6

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