Three-component one-pot reaction for the synthesis of β-amide ketones

被引：3
|
作者：
Luo, Yan-Ping [1 ]
Chen, Qiong [2 ]
机构：
[1] Hainan Univ, Key Lab Protect & Dev Utilisat Trop Crop Germplas, Minist Educ, Haikou 570228, Peoples R China
[2] Cent China Normal Univ, Key Lab Pesticide & Chem Biol, Minist Educ, Coll Chem, Wuhan 430079, Peoples R China
来源：
CHEMICAL PAPERS | 2013年 / 67卷 / 05期
基金：
中国国家自然科学基金;
关键词：
beta-amide ketones; one-pot reaction; synthesis; DAKIN-WEST REACTION; ACETAMIDO KETONES; EFFICIENT; CATALYST; PROPARGYLAMINES; ALDEHYDES; ALKYNES; ACIDS;
D O I：
10.2478/s11696-013-0313-0
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
beta-amide ketones were synthesised by a three-component one-pot reaction of phenylacetylene, aldehydes, and amides in anhydrous acetonitrile containing trifluoroacetic acid and acetic acid in the presence of AlCl3 catalyst. The title compound structures were identified by H-1 NMR, C-13 NMR, MS, and elemental analysis.
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页码：532 / 537
页数：6
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