Solvent-free Synthesis of Dihydrofuran-fused [60]Fullerene Derivatives by High-speed Vibration Milling

被引：0
|
作者：
Yasujiro MURATA
Koichi KOMATSU
机构：
[1] Institute for Chemical Research
[2] Japan
[3] Kyoto 611-0011
[4] Kyoto University
[5] Uji
来源：
ChineseChemicalLetters | 2005年 / 10期
关键词：
60]Fullerene; mechanochemical; solvent-free; β-dicarbonyl compounds;
D O I：
暂无
中图分类号：
O621.2 [有机化合物性质];
学科分类号：
070303 ; 081704 ;
摘要：
Solvent-free reactions of 1, 3-cyclohexanedione, 5, 5-dimethyl-1, 3-cyclohexanedione, 2, 4-pentanedione and ethyl acetoacetate with C60 in the presence of Mn(OAc)3·2H2O and ceric ammonium nitrate (CAN) under the high-speed vibration milling conditions afforded dihydrofuran-fused C60 derivatives. CAN is the better oxidant than Mn(OAc)3·2H2O in these mechanochemical reactions.
引用
收藏
页码：1327 / 1329
页数：3
相关论文
共 50 条
  • [41] Synthesis of Pyrroles from β-Enamines and Nitroolefins Catalyzed by I2 under High-speed Vibration Milling (HSVM)
    Xu, Hui
    Li, Yujin
    Xing, Mengming
    Jia, Jianhong
    Han, Liang
    Ye, Qing
    Gao, Jianrong
    CHEMISTRY LETTERS, 2015, 44 (04) : 574 - 576
  • [42] Nano TiO2@KSF as a high-efficient catalyst for solvent-free synthesis of Biscoumarin derivatives
    Zeydi, Masoud Mohammadi
    Mahmoodi, Nosratollah
    INTERNATIONAL JOURNAL OF NANO DIMENSION, 2016, 7 (02) : 174 - 180
  • [43] N-arylation of pyrrolidino[3′,4′:1,2][60]fullerene:: Synthesis under solvent-free conditions and electrochemistry of new C60-acceptor dyads
    de la Cruz, P
    de la Hoz, A
    Langa, F
    Martín, N
    Pérez, MC
    Sánchez, L
    EUROPEAN JOURNAL OF ORGANIC CHEMISTRY, 1999, 1999 (12) : 3433 - 3436
  • [44] An efficient catalyst- and solvent-free method for the synthesis of medicinally important dihydropyrano[2,3-c]pyrazole derivatives using ball milling technique
    Mohammad G. Dekamin
    Mohammad Alikhani
    Atefeh Emami
    Hossein Ghafuri
    Shahrzad Javanshir
    Journal of the Iranian Chemical Society, 2016, 13 : 591 - 596
  • [45] An efficient catalyst- and solvent-free method for the synthesis of medicinally important dihydropyrano[2,3-c]pyrazole derivatives using ball milling technique
    Dekamin, Mohammad G.
    Alikhani, Mohammad
    Emami, Atefeh
    Ghafuri, Hossein
    Javanshir, Shahrzad
    JOURNAL OF THE IRANIAN CHEMICAL SOCIETY, 2016, 13 (03) : 591 - 596
  • [46] A fast, simple and convenient procedure for the synthesis of fused pyrimidinone derivatives by using [Hmim][HSO4] as a green, efficient and reusable catalyst under solvent-free conditions
    Khazdooz, Leila
    Zarei, Amin
    Hajipour, Abdol Reza
    Sheikhan, Nafisehsadat
    IRANIAN JOURNAL OF CATALYSIS, 2012, 2 (04): : 173 - 178
  • [47] AlCl3-PROMOTED CYCLIZATION OF β-KETO DERIVATIVES WITH IN SITU GENERATED ENAMINES UNDER SOLVENT-FREE HIGH SPEED BALL MILLING: AN EFFICIENT ONE-POT ACCESS TO POLYSUBSTITUTED 1,4-DIHYDROPYRIDINES
    Zeng, Ji-Chao
    Yu, Fei
    Asiri, Abdullah M.
    Marwani, Hadi M.
    Zhang, Ze
    HETEROCYCLES, 2017, 94 (11) : 2054 - 2064
  • [48] Green Synthesis of Fused Imidazo[1,2-a][1,8]naphthyridine Derivatives Catalyzed by DABCO under Solvent-Free Solid-State Conditions and Their Biological Evaluation
    Banoth, Sonyanaik
    Perugu, Shyam
    Boda, Sakram
    JOURNAL OF HETEROCYCLIC CHEMISTRY, 2018, 55 (03) : 709 - 715
  • [49] Conventional and microwave-assisted solvent-free synthesis of fused [1,2,5]thiadiazolo[3,4-b]quinoxaline-2,2-dioxide derivatives
    Dehamchia, Mohamed
    Regainia, Zine
    JOURNAL OF SULFUR CHEMISTRY, 2013, 34 (03) : 242 - 249
  • [50] Fast, solvent-free, highly enantioselective three-component coupling of aldehydes, alkynes, and amines catalysed by the copper(II)pybox complex under high-vibration ball-milling
    Li, Zhenhua
    Jiang, Zhijiang
    Su, Weike
    GREEN CHEMISTRY, 2015, 17 (04) : 2330 - 2334
12345