Solvent-free Synthesis of Dihydrofuran-fused [60]Fullerene Derivatives by High-speed Vibration Milling

被引：0
|
作者：
Yasujiro MURATA
Koichi KOMATSU
机构：
[1] Institute for Chemical Research
[2] Japan
[3] Kyoto 611-0011
[4] Kyoto University
[5] Uji
来源：
ChineseChemicalLetters | 2005年 / 10期
关键词：
60]Fullerene; mechanochemical; solvent-free; β-dicarbonyl compounds;
D O I：
暂无
中图分类号：
O621.2 [有机化合物性质];
学科分类号：
070303 ; 081704 ;
摘要：
Solvent-free reactions of 1, 3-cyclohexanedione, 5, 5-dimethyl-1, 3-cyclohexanedione, 2, 4-pentanedione and ethyl acetoacetate with C60 in the presence of Mn(OAc)3·2H2O and ceric ammonium nitrate (CAN) under the high-speed vibration milling conditions afforded dihydrofuran-fused C60 derivatives. CAN is the better oxidant than Mn(OAc)3·2H2O in these mechanochemical reactions.
引用
收藏
页码：1327 / 1329
页数：3
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