5,10,15,20-TETRAKIS(P-CHLOROPHENYL)-PORPHYRIN

被引：12

作者：

HOKELEK, T ^{[1
]}

ULKU, D ^{[1
]}

GUNDUZ, N ^{[1
]}

HAYVALI, M ^{[1
]}

KILIC, Z ^{[1
]}

机构：

[1] UNIV ANKARA,DEPT CHEM,ANKARA,TURKEY

来源：

ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS | 1993年 / 49卷

关键词：

D O I：

10.1107/S0108270193000782

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

The title molecule, 2,7,12,17-tetrakis(4-chloro-phenyl)-21,22,23,24-tetraazapentacyclo[I 6.2. 1.1(3,6.-1(8,11.)1(13,16]tetracosa-1,3(22),4,6,8,10,12,14,16(4),17,-19-undecaene, is crystallographically centrosymmetric and the dihedral angle between the two pyrrole ring planes is 5.0 (4)-degrees . The molecular structure is a consequence of steric hinderances between the a-H atoms of the pyrrole and the ortho-H atoms of the phenyl rings. The dihedral angles between the pyrrole and phenyl rings are 54.8 (4) and 111. 1 (3)-degrees, respectively. The sums of the angles around meso-C atoms are -360-degrees and the average bond length between meso and adjacent macrocyclic ring C atoms is 1.398 (6) angstrom.

引用

页码：1667 / 1670

页数：4

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