N-3-oxoalkylamides and -thioamide in the synthesis of heterocyclic compounds. Part 1. Synthesis of 1,1-diethoxy-3-isothiocyanatobutane and reactions based on it

被引：6

作者：

Fisyuk A.S. ^{[1
]}

Berdovich L.V. ^{[1
]}

Temnikov D.V. ^{[1
]}

Knyaz'kova L.N. ^{[1
]}

机构：

[1] Omsk State University

来源：

Chemistry of Heterocyclic Compounds | 1997年 / 33卷 / 7期

基金：

俄罗斯基础研究基金会;

关键词：

Ethyl; Organic Chemistry; Heterocyclic Compound; Thione; Thioamides;

D O I：

10.1007/BF02253030

中图分类号：

学科分类号：

摘要：

The reaction of 3-isothiocyanatobutanal with ethanol in the presence of ethyl orthoformate produced 1,1-diethoxy-3-isothiocyanatobutane. The latter was used to devise methods of preparing 3-methylaminobutanal diethylacetal, N-(4-diethoxybutyl-2)thioamides, N-(4-oxybutyl-2)-thioamides, and 6-methyl-3-phenyl-5,6-di-hydropyridine-2(1H)-thione. ©1998 Plenum Publishing Corporation.

引用

页码：805 / 810

页数：5

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[1] N-3-oxoalkylamides and -thioamide in the synthesis of heterocyclic compounds. Part 1. Synthesis of 1,1-diethoxy-3-isothiocyanatobutane and reactions based on it
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[2] N-3-Oxoalkylamides and -thioamides in synthesis of heterocyclic compounds .1. Synthesis of 1,1-diethoxy-3-isothiocyanatobutane and reactions on its basis
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