N-3-oxoalkylamides and -thioamide in the synthesis of heterocyclic compounds. Part 1. Synthesis of 1,1-diethoxy-3-isothiocyanatobutane and reactions based on it

被引：6
|
作者：
Fisyuk A.S. [1 ]
Berdovich L.V. [1 ]
Temnikov D.V. [1 ]
Knyaz'kova L.N. [1 ]
机构：
[1] Omsk State University
来源：
Chemistry of Heterocyclic Compounds | 1997年 / 33卷 / 7期
基金：
俄罗斯基础研究基金会;
关键词：
Ethyl; Organic Chemistry; Heterocyclic Compound; Thione; Thioamides;
D O I：
10.1007/BF02253030
中图分类号：
学科分类号：
摘要：
The reaction of 3-isothiocyanatobutanal with ethanol in the presence of ethyl orthoformate produced 1,1-diethoxy-3-isothiocyanatobutane. The latter was used to devise methods of preparing 3-methylaminobutanal diethylacetal, N-(4-diethoxybutyl-2)thioamides, N-(4-oxybutyl-2)-thioamides, and 6-methyl-3-phenyl-5,6-di-hydropyridine-2(1H)-thione. ©1998 Plenum Publishing Corporation.
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页码：805 / 810
页数：5
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