Synthesis and Crystal Structure of 1-(2-Fluorophenyl)-3-(1H-1,2,4-triazol-1-yl)propan-1-one

被引：0
|
作者：
Zeng, Wulan [1 ]
Wang, Lintong [1 ]
Guo, Huanmei [1 ]
Jian, Fangfang [1 ]
机构：
[1] Weifang Univ, MicroScale Sci Inst, Dept Chem & Chem Engn, Weifang 261061, Peoples R China
来源：
ASIAN JOURNAL OF CHEMISTRY | 2010年 / 22卷 / 08期
关键词：
Synthesis; Crystal structure; 1-(2-Fluorophenyl)-3-(1H-1,2,4-triazol-1-yl)propan-1-one; BIOLOGICAL-ACTIVITIES;
D O I：
暂无
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
The compound 1-(2-fluorophenyl)-3-(1H-1,2,4-triazol-1-yl)propan-1-one, was synthesized and characterized by means of elemental analysis, IR spectrum and X-ray diffraction. It crystallizes in monoclinic, space group P2(1)/c with a = 11.757(15), b = 4.904(6), c = 21.50(3) angstrom, beta = 118.11(6)degrees, C(11)H(10)N(3)OF, M(r) = 219.21, V = 1093(2)angstrom(3), Z = 4, Dc = 1.326 g/cm(3), F(000) = 452, mu = 0.101 mm(-1), final R(1) = 0.1101. The triazole ring and 2-fluorophenyl ring makes dihedral angles of 85.97 degrees. There is obvious potentially weak intra- and intermolecular C-H center dot center dot center dot O hydrogen bonds in the crystal, which stabilizes the crystal structure.
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收藏
页码：6185 / 6189
页数：5
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