N-acetyl-N′-{3-cyano-1-[2,6-dichloro-4-(trifluoromethyl)phenyl]pyrazol-5-yl}thiourea

被引：2
|
作者：
Zhang, Xiao-Hong [1 ]
Zhong, Ping [1 ]
Lin, Qiao-Ying [1 ]
机构：
[1] Wenzhou Univ, Coll Chem & Mat Sci, Wenzhou 325027, Peoples R China
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2007年 / 63卷
关键词：
D O I：
10.1107/S1600536807020715
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
In the title molecule, C14H8Cl2F3N5OS, all bond lengths and angles are normal. Intramolecular N-H center dot center dot center dot O hydrogen bonding influences the molecular conformation. The pyrazole and benzene rings make a dihedral angle of 72.5 ( 1) degrees. Weak intermolecular N-H center dot center dot center dot S hydrogen bonds link the molecules into centrosymmetric dimers.
引用
收藏
页码：O3077 / U2345
页数：9
相关论文
共 50 条
  • [41] 4-Bromo-5-[(4-chlorobenzylidene)-amino]-1-[2,6-dichloro-4-(trifluoromethyl)phenyl]-1H-pyrazole-3-carbonitrile
    Yu, Xiao-Chun
    Li, Shu-Yan
    Zhong, Ping
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2007, 63 : O3098 - U2531
  • [42] 4-bromo-1-[2,6-dichloro-4-(trifluoromethyl)-phenyl]-5-[(2-furyl) methyleneamino]-1H-pyrazole-3-carbonitrile
    Li, Shu-Yan
    Zhong, Ping
    Hu, Mao-Lin
    Li, Jin-Hai
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2006, 62 : O4499 - O4500
  • [43] 1-[2,6-Dichloro-4-(trifluoromethyl)phenyl]-5-[(3,4-methylenedioxyphenyl)methyleneimino]-1H-pyrazole-3-carbonitrile
    Zhong, P
    Zhang, XH
    Yang, ZP
    Xiao, HP
    Hu, ML
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2005, 61 : O1448 - O1449
  • [44] 5-[(2-benzylideneethyl-idene)amino]-1-[2,6-dichloro-4-(trifluoromethyl)phenyl]-1H-pyrazole-3-carbonitrile
    Li, Shu-Yan
    Zhong, Ping
    Hu, Mao-Lin
    Luo, Yi
    Li, Jin-Hai
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2006, 62 : O2333 - O2334
  • [45] Synthesis and reactivity of N-[3-amino-4-(benzoxazol-2-yl)pyrazol-5-yl]phenylamine
    Abdelhamid, Abdou O.
    Baghos, Victorin B.
    Halim, Mervat M. A.
    JOURNAL OF CHEMICAL RESEARCH, 2007, (07) : 420 - 425
  • [46] Crystal structure of 1-(2,6-dichloro-4-(trifluoromethyl)phenyl)-5-((4-trifluoromethyl)methyleneimino)-1H-pyrazole-3-carbonitrile, C19H8Cl2F6N4
    Zhang, Xing-Guo
    Chen, Mu-Wang
    Hu, Mao-Lin
    Zhong, Ping
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2007, 222 (03): : 257 - 258
  • [47] (E)-1-[2,6-dichloro-4-(trifluoromethyl)-phenyl]-5-[(dimethylamino)methyleneamino]-1H-pyrazole-4-carboxylic acid
    Xie, De-Ming
    Shu, Zhan
    Shen, Liang
    Ding, Zhe-Wu
    Jin, Zhi-Min
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2007, 63 : O4562 - U3701
  • [48] 1-[2,6-Dichloro-4-(trifluoromethyl)phenyl]-5-(2,5-dioxo-2,5-dihydro-1H-pyrrol-1-yl)-1H-pyrazole-3-carbonitrile
    Yang, ZP
    Zhong, P
    Hu, ML
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2004, 60 : O1351 - O1352
  • [49] Crystal structure of 1-(2,6-dichloro-4-(trifluoromethyl)phenyl)-5-((3-bromo-phenyl)methyleneimino)-IH-pyrazole-3-carbonitrile, C18H8BrCl2F3N4
    Zhang, X-G.
    Zhang, X. -H.
    Zhong, P.
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2006, 221 (04): : 535 - 536
  • [50] 4-(5-Phenyl-3-trifluoromethyl-1H-pyrazol-1-yl)benzenesulfonamide
    Asiri, Abdullah M.
    Al-Youbi, Abdulrahman O.
    Faidallah, Hassan M.
    Ng, Seik Weng
    Tiekink, Edward R. T.
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : O2424 - U1087
12345