N-acetyl-N′-{3-cyano-1-[2,6-dichloro-4-(trifluoromethyl)phenyl]pyrazol-5-yl}thiourea

被引：2
|
作者：
Zhang, Xiao-Hong [1 ]
Zhong, Ping [1 ]
Lin, Qiao-Ying [1 ]
机构：
[1] Wenzhou Univ, Coll Chem & Mat Sci, Wenzhou 325027, Peoples R China
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2007年 / 63卷
关键词：
D O I：
10.1107/S1600536807020715
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
In the title molecule, C14H8Cl2F3N5OS, all bond lengths and angles are normal. Intramolecular N-H center dot center dot center dot O hydrogen bonding influences the molecular conformation. The pyrazole and benzene rings make a dihedral angle of 72.5 ( 1) degrees. Weak intermolecular N-H center dot center dot center dot S hydrogen bonds link the molecules into centrosymmetric dimers.
引用
收藏
页码：O3077 / U2345
页数：9
相关论文
共 50 条
  • [21] 1-[2,6-dichloro-4-(trifluoromethyl)phenyl]-5-(phenyl-acetamido)1H-pyrazole-3-carbonitrile
    Zhang, XH
    Chen, JZ
    Zhong, P
    Xiao, HP
    Hu, ML
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2005, 61 : O3676 - O3678
  • [22] 5-Amino-1-[2,6-dichloro-4-(trifluoromethyl)-phenyl]-4-(trifluoromethylsulfanyl)-1H-pyrazole-3-carbonitrile
    Tang, RY
    Zhong, P
    Lin, QL
    Hu, ML
    Shi, Q
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2005, 61 : O4374 - O4375
  • [23] 2-Chloro-N-[3-cyano-1-(3,4- dichlorophenyl)-1H-pyrazol-5-yl]acetamide
    Li, Ming
    Zhu, Jing
    Wei, Hong-xia
    Wang, Jian-qiang
    Guo, Cheng
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : O1150 - +
  • [24] 1-[2,6-dichloro-4-(trifluoromethyl)phenyl]-5-(4-methylphenylsulfonamido)-1H-pyrazole-3-carbonitrile
    Zhong, P
    Zhang, XH
    Xiao, HP
    Hu, ML
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2006, 62 : O513 - O515
  • [25] 1-[2,6-dichloro-4-(trifluoromethyl)phenyl]5-[(dimethylsulfonyl)amino]-1H-pyrazole-3-carbonitrile
    Yang, ZP
    Zhong, P
    Hu, ML
    Li, SY
    Tang, RY
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2005, 61 : O116 - O117
  • [26] N-[(5-Chloro-3-methyl-1-phenyl-1H-pyrazol-4-yl)carbonyl]-N′-(4-hydroxy-phenyl)thiourea
    Du, Haitang
    Du, Haijun
    An, Ying
    Li, Shengnan
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2008, 64 : O1404 - U1477
  • [27] 5-(2-Chlorobenzamido)-1-[2,6-dichloro-4-(trifluoromethyl)phenyl]-1H-pyrazole-3-carbonitrile
    Zhang, XH
    Zhong, P
    Yang, ZP
    Hu, ML
    Xiao, HP
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2005, 61 : O806 - O807
  • [28] N-(5-Chloro-3-methyl-1-phenyl-1H-pyrazol-4-ylcarbonyl)-N′-(2,6-dimethylphenyl) thiourea
    Du, Hai-Tang
    Du, Hai-Jun
    Lu, Ming
    Sun, Li-Li
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2008, 64 : O157 - U3924
  • [29] 1-[2,6-dichloro-4-(trifluoromethyl)phenyl]-5-[(4-methylbenzylidene)amino]-1H-pyrazole-3-carbonitrile
    Zhong, P
    Yang, Z
    Shi, Q
    Li, S
    Tang, R
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2005, 61 : O559 - O560
  • [30] 5-(3-Bromobenzylideneamino)-4-chloro-1-[2,6-dichloro-4-(trifluoromethyl)phenyl]-1H-pyrazole-3-carbonitrile
    Li, Shu-Yan
    Zhong, Ping
    Hu, Mao-Lin
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2006, 62 : O2832 - O2833
12345