N-acetyl-N′-{3-cyano-1-[2,6-dichloro-4-(trifluoromethyl)phenyl]pyrazol-5-yl}thiourea

被引：2
|
作者：
Zhang, Xiao-Hong [1 ]
Zhong, Ping [1 ]
Lin, Qiao-Ying [1 ]
机构：
[1] Wenzhou Univ, Coll Chem & Mat Sci, Wenzhou 325027, Peoples R China
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2007年 / 63卷
关键词：
D O I：
10.1107/S1600536807020715
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
In the title molecule, C14H8Cl2F3N5OS, all bond lengths and angles are normal. Intramolecular N-H center dot center dot center dot O hydrogen bonding influences the molecular conformation. The pyrazole and benzene rings make a dihedral angle of 72.5 ( 1) degrees. Weak intermolecular N-H center dot center dot center dot S hydrogen bonds link the molecules into centrosymmetric dimers.
引用
收藏
页码：O3077 / U2345
页数：9
相关论文
共 50 条
  • [31] 1-[2,6-Dichloro-4-(trifluoromethyl)phenyl]-5-[(4-nitrophenyl)methyleneimino]-1H-pyrazole-3-carbonitrile
    Zhong, P
    Yang, ZP
    Shi, Q
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2005, 61 : O786 - O787
  • [32] 1-[2,6-Dichloro-4-(trifluoromethyl)phenyl]-5-[(2-hydroxybenzylidene)amino]-1H-pyrazole-3-carbonitrile
    Yang, ZP
    Zhong, P
    Shi, Q
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2006, 62 : O783 - O784
  • [33] 1-[2,6-dichloro-4-(trifluoromethyl)phenyl]-5-[(4-dimethylaminobenzylidene)amino]-1H-pyrazole-3-carbonitrile
    Chen, D
    Yang, Z
    Zhong, P
    Hu, M
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2005, 61 : O702 - O703
  • [34] 5-[(4-bromophenyl) methyleneimino]-1-[2,6-dichloro-4-(trifluoromethyl) phenyl]-1H-pyrazole-3-carbonitrile
    Li, Shu-Yan
    Zhong, Ping
    Hu, Mao-Lin
    Luo, Yi
    Li, Jin-Hai
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2006, 62 : O3821 - O3822
  • [35] 1-[2,6-Dichloro-4-(trifluoromethyl)phenyl]-5-[(4-methoxyphenyl) methyleneimino]-1H-pyrazole-3-carbonitrile
    Zhang, XH
    Yang, ZP
    Zhong, P
    Hu, ML
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2005, 61 : O908 - O909
  • [36] 5-(2,4-dichlorobenzamido)-1-[2,6-dichloro-4-(trifluoromethyl) phenyl]-1H-pyrazole-3-carbonitrile
    Zhong, P
    Zhang, XH
    Xiao, HP
    Hu, ML
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2005, 61 : O3110 - O3111
  • [37] 4-chloro-1-[2,6-dichloro-4-(trifluoromethyl)phenyl]-5-(4-methylbenzylideneamino)-1H-pyrazole-3-carbonitrile
    Li, Shu-Yan
    Zhong, Ping
    Hu, Mao-Lin
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2006, 62 : O2113 - O2114
  • [38] 1-[2,6-Dichloro-4-(trifluoromethyl) phenyl]-5-[(2-furyl) methyleneamino]-1H-pyrazole-3-carbonitrile
    Zhong, P
    Yang, ZP
    Shi, Q
    Hu, ML
    Li, SY
    Tang, RY
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2005, 61 : O2972 - O2973
  • [39] 1-[2,6-Dichloro-4-(trifluoromethyl)-phenyl]-3,4-dimethylpyrano[2,3-c]-pyrazol-6(1H)-one
    Fun, Hoong-Kun
    Loh, Wan-Sin
    Sarojini, B. K.
    Mohan, B. J.
    Narayana, B.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : 02350 - +
  • [40] 5-{[(4-Chlorophenyl)methylene]amino}1-[2,6-dichloro-4-(trifluoromethyl)phenyl]1H-pyrazole-3-carbonitrile
    Yang, ZP
    Zhong, P
    Shi, Q
    Tang, RY
    Li, SY
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2005, 61 : O949 - O950
12345