N-acetyl-N′-{3-cyano-1-[2,6-dichloro-4-(trifluoromethyl)phenyl]pyrazol-5-yl}thiourea

被引：2
|
作者：
Zhang, Xiao-Hong [1 ]
Zhong, Ping [1 ]
Lin, Qiao-Ying [1 ]
机构：
[1] Wenzhou Univ, Coll Chem & Mat Sci, Wenzhou 325027, Peoples R China
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2007年 / 63卷
关键词：
D O I：
10.1107/S1600536807020715
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
In the title molecule, C14H8Cl2F3N5OS, all bond lengths and angles are normal. Intramolecular N-H center dot center dot center dot O hydrogen bonding influences the molecular conformation. The pyrazole and benzene rings make a dihedral angle of 72.5 ( 1) degrees. Weak intermolecular N-H center dot center dot center dot S hydrogen bonds link the molecules into centrosymmetric dimers.
引用
收藏
页码：O3077 / U2345
页数：9
相关论文
共 50 条
  • [1] N-{3-cyano-1-[2,6-dichloro-4-(trifluoromethyl)-phenyl]-1H-pyrazol-5-yl}benzamide
    Zhong, P
    Yang, ZP
    Li, SY
    Tang, RY
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2004, 60 : O2395 - O2396
  • [2] N-{3-cyano-1-[2,6-dichloro-4-(trifluoromethyl)phenyl]-1H-pyrazol-5-yl}acetamide
    Yang, ZP
    Zhong, P
    Guo, SR
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2004, 60 : O1277 - O1278
  • [3] 2-Chloro-N-{3-cyano-1-[2,6-dichloro-4-(trifluoromethyl)phenyl]-1H-pyrazol-5-yl}acetamide
    Zhang, Jian-qiang
    He, Qiu
    Jiang, Qiang-hua
    Mu, Hai-pin
    Wan, Rong
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2012, 68 : o104
  • [4] N-{3-Cyano-1-[2,6-dichloro-4-(trifluoromethyl)phenyl]-1H-pyrazol-5-yl}-4-nitrobenzamide ethanol solvate
    Zhong, P
    Yang, ZP
    Shi, Q
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2005, 61 : O841 - O842
  • [5] N,N′-Bis{3-cyano-1-[2,6-dichloro-4(trifluoromethyl)phenyl]-1H-pyrazol-5-yl}-1,4-benzenediamide dimethylformamide disolvate
    Chen, DM
    Zhong, P
    Yang, ZP
    Hu, ML
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2005, 61 : O1362 - O1363
  • [6] Synthesis, spectroscopic and crystal structure studies of N-{3-cyano-1-[2,6-dichloro-4-(trifluoromethyl)phenyl]-4-(ethylsulfanyl)-1H-pyrazol-5-yl}-2,2,2-trifluoroacetamide
    Priyanka, Prabhakar
    Jayanna, Bidarur K.
    Kumar, Yelekere C. Sunil
    Shreenivas, Mellekatte T.
    Srinivasa, Gejjelegere R.
    Divakara, Thayamma R.
    Yathirajan, Hemmige S.
    Parkin, Sean
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2022, 78 : 1084 - +
  • [7] Bis{5-amino-3-cyano-1-[2,6-dichloro-4-(trifluoromethyl)phenyl]-1H-pyrazol-4-yl} disulfide acetonitrile disolvate
    Tang, RY
    Zhong, P
    Li, SY
    Hu, ML
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2005, 61 : O1564 - O1565
  • [8] 2-(4-chlorophenyl)-N-{3-cyano-1-[2,6-dichloro4-(trifluoromethyl)phenyl]-1H-pyrazol-5-yl}3-methylbutanamide ethanol solvate
    Cheng, JL
    Wei, FL
    Gui, WJ
    Zhu, GN
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2006, 62 : O1836 - O1838
  • [9] X-ray diffraction, DFT, spectroscopic study and insecticidal activity of (3-cyano-1-(2,6-dichloro-4-(trifluoromethyl)phenyl)-4-((trifluoromethyl)sulfinyl)-1H-pyrazol-5-yl)(2-(triethylammonio)acetyl)amide inner salt
    D. X. Jiang
    X. H. Zheng
    H. H. Xu
    N. B. Wong
    Crystallography Reports, 2014, 59 : 1078 - 1083
  • [10] X-ray diffraction, DFT, spectroscopic study and insecticidal activity of (3-cyano-1-(2,6-dichloro-4-(trifluoromethyl)phenyl)-4-((trifluoromethyl)sulfinyl)-1H-pyrazol-5-yl)(2-(triethylammonio)acetyl)amide inner salt
    Jiang, D. X.
    Zheng, X. H.
    Xu, H. H.
    Wong, N. B.
    CRYSTALLOGRAPHY REPORTS, 2014, 59 (07) : 1078 - 1083
12345