Dynamic ligand-exchange chiral stationary phase derived from aminoalcohol

被引:0
|
作者
Sliwka, M [1 ]
Slebioda, M [1 ]
Kolodziejczyk, AM [1 ]
机构
[1] Gdansk Tech Univ, Dept Organ Chem, PL-80952 Gdansk, Poland
来源
CHEMIA ANALITYCZNA | 1997年 / 42卷 / 06期
关键词
ligand-exchange chromatography; enantiomeric separation; chiral stationary phase;
D O I
暂无
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
The chiral ligand-exchange stationary phase based on N-alkylphenylglycinol was synthesised and dynamically loaded onto octadecyl-silica. Efficiency of the chiral column and influence of various factors (concentration of copper (IT) ions, pH of the mobile phase, column temperature and organic modifier addition) on separation of enatiomers of alpha-amino acids were evaluated.
引用
收藏
页码:895 / 900
页数:6
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