HIGH-PERFORMANCE LIGAND-EXCHANGE CHROMATOGRAPHY OF AMINO ACIDS ON CHIRAL STATIONARY PHASES.

被引：0
|
作者：
Carunchio, V. [1 ]
Messina, A. [1 ]
Sinibaldi, M. [1 ]
Fanali, S. [1 ]
机构：
[1] Univ 'La Sapienza', Rome, Italy, Univ 'La Sapienza', Rome, Italy
来源：
HRC & CC. Journal of high resolution chromatography & chromatography communications | 1988年 / 11卷 / 05期
关键词：
CHROMATOGRAPHIC ANALYSIS - Liquid - SILICA GEL;
D O I：
暂无
中图分类号：
学科分类号：
摘要：
Three chiral stationary phases, obtained by grafting silica gel with (-)-trans-1,2-cyclohexanediamine, were studied for the resolution of alpha -amino acids by ligand-exchange chromatography. The packings were prepared by bonding the chiral ligand to silica gel via different hydrocarbon spacers. Separation of the optical isomers was accomplished by eluents containing a constant concentration of copper(II) acetate (0. 05mM). The elution sequence of amino acids was found to be dependent on the grafting reaction selected to prepare the chiral packings.
引用
收藏
页码：401 / 404
相关论文
共 50 条
  • [1] HIGH-PERFORMANCE LIGAND-EXCHANGE CHROMATOGRAPHY OF AMINO-ACIDS ON CHIRAL STATIONARY PHASES
    CARUNCHIO, V
    MESSINA, A
    SINIBALDI, M
    FANALI, S
    JOURNAL OF HIGH RESOLUTION CHROMATOGRAPHY & CHROMATOGRAPHY COMMUNICATIONS, 1988, 11 (05): : 401 - 404
  • [2] NOVEL CHIRAL STATIONARY PHASES FOR THE RESOLUTION OF THE ENANTIOMERS OF AMINO-ACIDS BY LIGAND-EXCHANGE CHROMATOGRAPHY
    YUKI, Y
    SAIGO, K
    TACHIBANA, K
    HASEGAWA, M
    CHEMISTRY LETTERS, 1986, (08) : 1347 - 1350
  • [3] NOVEL CHIRAL STATIONARY PHASES FOR OPTICAL RESOLUTION BY LIGAND-EXCHANGE HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY
    YUKI, Y
    SAIGO, K
    KIMOTO, H
    TACHIBANA, K
    HASEGAWA, M
    JOURNAL OF CHROMATOGRAPHY, 1987, 400 : 65 - 75
  • [4] DIRECT SEPARATION OF AMINO ENANTIOMERS BY HIGH-PERFORMANCE LIGAND-EXCHANGE CHROMATOGRAPHY ON CHEMICALLY BONDED CHIRAL PHASES
    GUBITZ, G
    JUFFMANN, F
    JELLENZ, W
    CHROMATOGRAPHIA, 1982, 16 : 103 - 106
  • [5] HIGH-PERFORMANCE LIGAND-EXCHANGE CHROMATOGRAPHY OF SOME AMINO-ACIDS CONTAINING 2 CHIRAL CENTERS
    GALUSHKO, SV
    SHISHKINA, IP
    SOLOSHONOK, VA
    JOURNAL OF CHROMATOGRAPHY, 1992, 592 (1-2): : 345 - 348
  • [6] A NOVEL CHIRAL STATIONARY PHASE FOR OPTICAL RESOLUTION OF AMINO-ACIDS AND THEIR DERIVATIVES BY LIGAND-EXCHANGE HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY
    SAIGO, K
    YUKI, Y
    KIMOTO, H
    NISHIDA, T
    HASEGAWA, M
    BULLETIN OF THE CHEMICAL SOCIETY OF JAPAN, 1988, 61 (01) : 322 - 324
  • [7] Enantiomeric separation of non-protein amino acids by chiral ligand-exchange high-performance liquid chromatography
    Miyazawa, T
    Minowa, H
    Imagawa, K
    Yamada, T
    ANALYTICAL LETTERS, 1997, 30 (04) : 867 - 882
  • [8] DIRECT SEPARATION OF ENANTIOMERS BY HIGH-PERFORMANCE LIGAND-EXCHANGE CHROMATOGRAPHY ON CHEMICALLY BONDED CHIRAL PHASES
    GUBITZ, G
    JOURNAL OF LIQUID CHROMATOGRAPHY, 1986, 9 (2-3): : 519 - 535
  • [9] HIGH-PERFORMANCE LIGAND-EXCHANGE CHROMATOGRAPHY
    KARGER, BL
    ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 1982, 183 (MAR): : 97 - ANYL
  • [10] Separation of enantiomers of non-protein amino acids by high-performance liquid chromatography on a chiral ligand-exchange column
    Miyazawa, T
    Minowa, H
    Imagawa, K
    Yamada, T
    CHROMATOGRAPHIA, 2004, 60 (1-2) : 45 - 50
12345