{3,3′,5,5′-Tetramethoxy-2,2′-[ethane-1,2-diylbis(nitrilomethylidyne)]diphenolato}nickel(II)

被引：6
|
作者：
Assey, Gervas E. [1 ]
Butcher, Ray J. [1 ]
Gultneh, Yilma [1 ]
机构：
[1] Howard Univ, Dept Chem, Washington, DC 20059 USA
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2010年 / 66卷
关键词：
SCHIFF-BASE COMPLEXES; X-RAY; NICKEL(II); SUBSTITUENTS; OXIDATION; SALEN;
D O I：
10.1107/S1600536810016041
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
The title square-planar nickel complex, [Ni(C(20)H(22)N(2)O(6))],has Ni-N and Ni-O bond lengths of 1.8448 (14)/1.8478 (14) and 1.8536 (12)/1.8520 (12) angstrom. There is a slight twist in the two benzene rings at each end of the complex [dihedral angle = 11.11 (5)degrees]. All the atoms of the methoxy substitutents are in the plane of the ring to which they are attached except for one which deviates slightly [0.365 (3) angstrom]. In the crystal, weak C-H center dot center dot center dot O intermolecular interactions connect the molecules.
引用
收藏
页码：M620 / U273
页数：11
相关论文
共 50 条
  • [21] Dipotassium hexakis({2,2′-[ethane-1,2-diylbis(nitrilomethylidyne)]diphenolatol nickel(II)) tetracyanonickelate(II) methanol hexasolvate dihydrate
    Skovsgaard, S
    Bond, AD
    McKenzie, CJ
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2005, 61 : M135 - M137
  • [22] {3,3′-[Ethane-1,2-diylbis(methylimino)]-bis(propane-1-thiolato)}nickel(II)
    Grapperhaus, Craig A.
    O'Toole, Martin G.
    Mashuta, Mark S.
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2007, 63 : M2281 - U317
  • [23] {2,2'-[Ethane-1,2-diylbis(nitrilomethanylylidene)] diphenolato} (isopropanolato)aluminium dichloromethane hemisolvate
    Zaitsev, Kirill V.
    Kuchuk, Ekaterina A.
    Karlov, Sergey S.
    Zaitseva, Galina S.
    Churakov, Andrei V.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2013, 69 : M631 - +
  • [24] Bis{μ-2,2′-[ethane-1,3-diylbis(nitrilomethylidyne)]diphenolato}dizinc(II)
    Odoko, M
    Tsuchida, N
    Okabe, N
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2006, 62 : M708 - M709
  • [25] Aqua(dicyanamido){μ-6,6′-dimethoxy-2,2′-[ethane-1,2-diylbis(nitrilomethylidyne)]diphenolato}copper(II)sodium(I)
    Shen, Yong-Miao
    Wang, Wei
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : M472 - U1155
  • [26] {6,6′-Dimethoxy-2,2′-[ethane-1,2-diylbis(nitrilomethanylylidene)]diphenolato}nickel(II) dimethylformamide monosolvate
    Ayikoe, Kouassi
    Butcher, Ray J.
    Gultneh, Yilma
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : M328 - U436
  • [27] Aqua{4,4′-dibromo-6,6′-dimethoxy-2,2′-[ethane-1,2-diylbis(nitrilomethylidyne)]diphenolato}copper(II)
    Xie, Hai
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : M1577 - U720
  • [28] Dichlorido{μ3-6,6′-diethoxy-2,2′-[ethane-1,2-diylbis(nitrilomethylidyne)]diphenolato}octamethyldi-μ3-oxido-tetratin(IV)
    Lee, See Mun
    Lo, Kong Mun
    Ng, Seik Weng
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : M1103 - U826
  • [29] COBALT(II), NICKEL(II) AND ZINC(II) COMPLEXES OF 3,3'-[ETHANE-1,2-DIYLBIS(IMINO)]BIS(PROPANAMIDE) IN SOLUTION
    LIM, MC
    AUSTRALIAN JOURNAL OF CHEMISTRY, 1983, 36 (01) : 19 - 24
  • [30] RETRACTED: Bis{μ-2,2′-[ethane-1,2-diylbis(nitrilomethylidyne)]diphenolato}bis[(thiocyanato-κN)iron(III)] (Retracted Article)
    Hao, Lujiang
    Mu, Chunhua
    Kong, Binbin
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2008, 64 : M1034 - U594
12345