{3,3′,5,5′-Tetramethoxy-2,2′-[ethane-1,2-diylbis(nitrilomethylidyne)]diphenolato}nickel(II)

被引：6

作者：

Assey, Gervas E. ^{[1
]}

Butcher, Ray J. ^{[1
]}

Gultneh, Yilma ^{[1
]}

机构：

[1] Howard Univ, Dept Chem, Washington, DC 20059 USA

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2010年 / 66卷

关键词：

SCHIFF-BASE COMPLEXES; X-RAY; NICKEL(II); SUBSTITUENTS; OXIDATION; SALEN;

D O I：

10.1107/S1600536810016041

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

The title square-planar nickel complex, [Ni(C(20)H(22)N(2)O(6))],has Ni-N and Ni-O bond lengths of 1.8448 (14)/1.8478 (14) and 1.8536 (12)/1.8520 (12) angstrom. There is a slight twist in the two benzene rings at each end of the complex [dihedral angle = 11.11 (5)degrees]. All the atoms of the methoxy substitutents are in the plane of the ring to which they are attached except for one which deviates slightly [0.365 (3) angstrom]. In the crystal, weak C-H center dot center dot center dot O intermolecular interactions connect the molecules.

引用

页码：M620 / U273

页数：11

共 50 条

[41] 4,4′-[Propane-1,2-diylbis(nitrilomethylidyne)]dibenzonitrile-4,4′-[ethane-1,2-diylbis(nitrilomethylidyne)]dibenzonitrile [0.796(2)/0.204 (2)]
Fun, Hoong-Kun
Kia, Reza
Kargar, Hadi
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2008, 64 : O2124 - U1981
[42] RETRACTED: μ-oxido-bis({4,4′-dibromo-2,2′-[ethane-1,2-diylbis(nitrilomethylidyne)]diphenolato} manganese(III)) (Retracted Article)
Liu, Ying
Dou, Jianmin
Niu, Meiju
Zhang, Xianxi
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2007, 63 : M2771 - U1298
[43] Di-μ2-cyanido-dicyanidobis{2,2′-[ethane-1,2-diylbis(nitrilomethylidyne)]diphenolato}(1,4,8,11-tetraazacyclotetradecane)dichromium(III)nickel(II) methanol disolvate
Wang, Shi
He, Wenrui
Ding, Xuehua
Huang, Wei
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : M661 - U625
[44] {6,6′-Dimethoxy-2,2′-[ethane-1,2-diylbis-(nitrilomethylidyne)]diphenolato} (ethanol)-dioxouranium(VI)
Senyuz, Nuray
Yuksektepe, Cigdem
Bati, Humeyra
Caliskan, Nezihe
Buyukgungor, Orhan
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2006, 62 : M3163 - M3164
[45] Tetraaquatetrakis{μ3-3,3′-[(E,E)-ethane-1,2-diylbis(nitrilomethylidyne)]benzene-1,2-diolato}octazinc(II) N,N-dimethylformamide hexasolvate
Xu, Qin-Juan
Lin, Li-Rong
Sun, Di
Huang, Rong-Bin
Zheng, Lan-Sun
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : M1559 - U581
[46] RETRACTED: μ-Oxido-bis({4,4′-dibromo-2,2′-[ethane-1,2-diylbis(nitrilomethylidyne)]diphenolato}chromium(III)) (Retracted Article)
Liu, Ying
Dou, Jianmin
Niu, Meiju
Zhang, Xianxi
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2007, 63 : M3032 - U1559
[47] The cocrystal {4,4′-dimethoxy-2,2′-[propane-1,2-diylbis(nitrilomethylidyne)]diphenolato}methanol(pyridine)manganese(III) hexafluoridophosphate-{4,4′-dimethoxy-2,2′-[ethane-1,2-diylbis(nitrilomethylidyne)]diphenolato}methanol(pyridine)manganese(III)hexafluoridophosphate(1/1)
Habibi, Mohammad Hossein
Askari, Elham
Chantrapromma, Suchada
Fun, Hoong-Kun
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2007, 63 : M2905 - U460
[48] Di-mu-oxido-bis({2,2'-[ethane-1,2-diylbis(nitrilomethanylylidene)] diphenolato}titanium(IV)) chloroform disolvate
Zaitsev, Kirill V.
Karlov, Sergey S.
Piskun, Yulia A.
Vasilenko, Irina V.
Churakov, Andrei V.
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2013, 69 : M635 - +
[49] {μ-6,6′-Diethoxy-2,2′-[ethane-1,2-diylbis(nitrilomethylidyne)]diphenolato}-trinitratopraseodymium(III)nickel(II) (Retraction of vol E63, pg m2093, 2007)
Sui, Li
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : E21 - E22
[50] {μ-6,6′-Diethoxy-2,2′-[ethane-1,2-diylbis(nitrilomethylidyne)]diphenolato}-trinitratoholmium(III)nickel(II) (Retraction of vol E64, pg m806, 2008)
Xiao, Fu
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : E21 - E22

← 1 2 3 4 5 →