Benzyl 2-{[2-(tert-butoxycarbonylamino)-4-methylpentanoyl]methylamino}-4-methylpentanoate

被引：7
|
作者：
Liao, Xiao-Jian
Xu, Wen-Jie
Xu, Shi-Hai [1 ]
Dong, Fang-Fang
机构：
[1] Jinan Univ, Dept Chem, Guangzhou 510632, Guangdong, Peoples R China
[2] Jinan Univ, Inst Hydrobiol, Guangzhou 510632, Guangdong, Peoples R China
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2007年 / 63卷
关键词：
D O I：
10.1107/S1600536807029418
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
The title compound, C25H40N2O5, was synthesized in 55.9% yield by condensation of N-methyl-L-leucine benzyl ester toluene sulfonic acid with tert-butoxycarbonyl-L-leucine at 273 K and its crystal structure determined. The dipeptide derivative conjugates through the amide linkage and includes two protecting groups, a tert-butyloxycarbonyl group at the C-tip and a benzyl group at the N-tip.
引用
收藏
页码：O3313 / U4398
页数：10
相关论文
共 50 条
  • [41] The synthesis and crystal structure of 2-[4(S)-4,5-dihydro-4-phenyl-2-oxazolinyl]-benzenamine, and 2-[4(S)-4,5-dihydro-4-benzyl-2-oxazolinyl]-benzenamine
    Mei, Luo
    Hai, Zhang Jia
    Hao, Yin
    Min, Pang Wei
    Liang, Hu Ke
    CRYSTALLOGRAPHY REPORTS, 2010, 55 (07) : 1217 - 1219
  • [42] Synthesis, Crystal Structure and Inhibitory Activities of 2-(N-Tert-Butoxycarbonylamino)Pyridine Derivatives
    Shi, Yun-Lian
    Nie, Xu-Liang
    Huang, Tao
    Shi, Ming-Zhu
    Peng, Da-Yong
    Ren, Xue-Xiang
    Shi, Xu-Gen
    Zhao, Ming-Yu
    Li, Bao-Tong
    JOURNAL OF CHEMICAL CRYSTALLOGRAPHY, 2021, 51 (02) : 155 - 160
  • [43] {4-bromo-2-[2-(methylamino)ethyliminomethyl]phenolato}thiocyanato-copper(II)
    Ma, Jun-Ying
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2008, 64 : M878 - U257
  • [44] VIBRATIONAL SPECTRA AND FORCE CONSTANTS OF ZN(NCO)4=2- ZN(NCS)4=2- AND ZN(NCSE)4=2-
    FORSTER, D
    HORROCKS, WD
    INORGANIC CHEMISTRY, 1967, 6 (02) : 339 - &
  • [45] 2-[4-(tert-butylsulfanyl)benzyl]-9,9-diethyl-9H-fluorene
    Fan, Jian-Dong
    Yu, Wen-Tao
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2007, 63 : o1243 - o1244
  • [46] (Z)-2-(2-Aminothiazol-1-ium-4-yl)2-(tert-butoxycarbonylmethoxyimino)acetate monohydrate
    Xiang-Wei Cheng
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2007, 63 : O3728 - U2304
  • [47] tert-Butyl 2-(4-chlorobenzoyl)-2-methylpropanoate
    Crosse, Chelsey M.
    Kelly, Emily C.
    Logue, Marshall W.
    Luck, Rudy L.
    Maass, John S.
    Mehne, Katlyn C.
    Pignotti, Louis R.
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : O493 - U3633
  • [48] Synthesis, characterisation and electrochemical investigation of phthalocyanines with pendant 4-{2-[2-(4-tert-butylphenoxy)ethoxy]ethoxy} substituents
    Acar, Irfan
    Topcu, Saim
    Biyiklioglu, Zekeriya
    Kantekin, Halit
    COLORATION TECHNOLOGY, 2013, 129 (04) : 259 - 266
  • [49] Methyl 2-acetamido-2-(4-hydroxy-2-methyl-1,3-dioxo-1,2,3,4-tetrahydroisoquinolin-4-yl)-4-methylpentanoate
    Fun, Hoong-Kun
    Quah, Ching Kheng
    Xu, Kai
    Zhang, Yan
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : O1710 - U891
  • [50] 2-[2-(dimethylamino)ethylammoniomethyl]-4-nitrophenolate
    Hazell, A
    Overgaard, J
    Lausen, SK
    Hu, HJ
    Khoo, LE
    ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1997, 53 : 640 - 641
12345