Benzyl 2-{[2-(tert-butoxycarbonylamino)-4-methylpentanoyl]methylamino}-4-methylpentanoate

被引:7
|
作者
Liao, Xiao-Jian
Xu, Wen-Jie
Xu, Shi-Hai [1 ]
Dong, Fang-Fang
机构
[1] Jinan Univ, Dept Chem, Guangzhou 510632, Guangdong, Peoples R China
[2] Jinan Univ, Inst Hydrobiol, Guangzhou 510632, Guangdong, Peoples R China
关键词
D O I
10.1107/S1600536807029418
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
The title compound, C25H40N2O5, was synthesized in 55.9% yield by condensation of N-methyl-L-leucine benzyl ester toluene sulfonic acid with tert-butoxycarbonyl-L-leucine at 273 K and its crystal structure determined. The dipeptide derivative conjugates through the amide linkage and includes two protecting groups, a tert-butyloxycarbonyl group at the C-tip and a benzyl group at the N-tip.
引用
收藏
页码:O3313 / U4398
页数:10
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