One-pot three-component reaction of C60, amino acid and fluorinted benzaldehyde to C60-pyrrolidine derivatives

被引：11
|
作者：
Wang, S
Zhang, JM
Song, LP
Jiang, H
Zhu, SZ
机构：
[1] Shanghai Univ, Dept Chem, Sch Sci, Shanghai 200436, Peoples R China
[2] Chinese Acad Sci, Shanghai Inst Organ Chem, State Key Lab Organofluorine Chem, Shanghai 200032, Peoples R China
来源：
JOURNAL OF FLUORINE CHEMISTRY | 2005年 / 126卷 / 03期
基金：
中国国家自然科学基金;
关键词：
C-60; amino acid; fluorinated benzaldehyde; 1,3-dipolar cycloaddition; C-60-pyrrolidines;
D O I：
10.1016/j.jfluchem.2004.12.018
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
A series of fluorinated 2,5-disubstituted C-60-pyrrolidine derivatives were synthesized via one-pot three-component reaction of C-60, amino acid and fluorinated benzaldehyde under reflux in toluene or microwave irradiation. The cis- and trans-isomers could be isolated by chromatography and fully confirmed by H-1 NMR. (c) 2005 Elsevier B.V. All rights reserved.
引用
收藏
页码：349 / 353
页数：5
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