Synthesis and structure of a new three-dimentional open-framework zinc phosphate with 12-membered ring channels

被引：0
|
作者：
Wang, C [1 ]
Li, J [1 ]
Wang, Y [1 ]
Wang, K [1 ]
Yu, J [1 ]
Xu, R [1 ]
机构：
[1] Jilin Univ, State Key Lab Inorgan Synth & Preparat Chem, Changchun 130023, Peoples R China
来源：
RECENT ADVANCES IN THE SCIENCE AND TECHNOLOGY OF ZEOLITES AND RELATED MATERIALS, PTS A - C | 2004年 / 154卷
关键词：
zinc phosphate; open framework; hydrothermal synthesis; structure;
D O I：
暂无
中图分类号：
O64 [物理化学（理论化学）、化学物理学];
学科分类号：
070304 ; 081704 ;
摘要：
A new three-dimensional zinc phosphate [Zn6P5O20](3-)center dot[C6N3H15](3+)center dot H2O (I) has been hydrothermally synthesized from a reaction system Zn(OAC)(2)-1-(2-aminoethyl)piperazine-H3PO4-H2O. Single crystal X-ray diffraction analysis shows that it crystallizes in the monoclinic space group C2/c (no. 15) with a=20.240(4), b=16.856(3), c=8.1541(16)angstrom, beta=111.02(3)degrees, V=2596.7(9)angstrom(3) and Z=4. Its structure consists of one dimensional 12-membered ring channels along the [001] direction.
引用
收藏
页码：1035 / 1040
页数：6
相关论文
共 50 条
  • [41] New Crystalline Layered Zinc Phosphate with 10-Membered-Ring Channels Perpendicular to Layers
    Liu, Lei
    Ferdov, Stanislav
    Coelho, Cristina
    Kong, Ying
    Mafra, Luis
    Li, Jin P.
    Dong, Jin X.
    Kolitsch, Uwe
    Ferreira, Rute A. Sa
    Tillmanns, Ekkehart
    Rocha, Joao
    Lin, Zhi
    INORGANIC CHEMISTRY, 2009, 48 (11) : 4598 - 4600
  • [42] Synthesis, structure, and polymorphism studies in amine-templated open-framework zinc phosphites
    Mandal, Sukhendu
    Natarajan, Srinivasan
    INORGANIC CHEMISTRY, 2008, 47 (12) : 5304 - 5313
  • [43] Syntheses and structures of two open-framework zinc phosphites with extra-large 24-ring channels
    Wang, Pei
    Wang, Guo-Ming
    Li, Jin-Hua
    Wang, Zong-Hua
    Wang, Ying-Xia
    Lin, Jian-Hua
    SOLID STATE SCIENCES, 2012, 14 (08) : 1030 - 1035
  • [44] Hydrothermal synthesis and characterization of new hybrid open-framework indium phosphate-oxalates
    Chen, ZX
    Weng, LH
    Chen, JX
    Zhao, DY
    CHINESE SCIENCE BULLETIN, 2004, 49 (07): : 658 - 664
  • [45] Hydrothermal synthesis and characterization of new hybrid open-framework indium phosphate-oxalates
    CHEN Zhenxia
    Chinese Science Bulletin, 2004, (07) : 658 - 664
  • [46] Hydrothemal synthesis of new hybrid large open-framework indium phosphate-oxalates
    Chen, Z
    Weng, L
    Chen, J
    Chen, M
    Zhao, D
    RECENT ADVANCES IN THE SCIENCE AND TECHNOLOGY OF ZEOLITES AND RELATED MATERIALS, PTS A - C, 2004, 154 : 1118 - 1123
  • [47] Synthesis and characterization of three open-framework zinc phosphites with (3,4)-connected frameworks
    Kang, Maoping
    Luo, Daibing
    Luo, Xiuchao
    Lin, Zhien
    SOLID STATE SCIENCES, 2011, 13 (08) : 1473 - 1477
  • [48] Ionothermal synthesis of a new open-framework zinc phosphite NIS-3 with low framework density
    Feng, Jing-Dong
    Shao, Kui-Zhan
    Tang, Shu-Wei
    Wang, Rong-Shun
    Su, Zhong-Min
    CRYSTENGCOMM, 2010, 12 (05): : 1401 - 1403
  • [49] The synthesis and crystal structure of a new open-framework zincophosphate UiO-17
    Kongshaug, KO
    Fjellvåg, H
    Lillerud, KP
    JOURNAL OF MATERIALS CHEMISTRY, 1999, 9 (12) : 3119 - 3123
  • [50] Hydrothermal synthesis and structure of three novel open-framework lanthanide sulfate-oxalates
    Li, Li
    Yu, Ranbo
    Wang, Dan
    Lai, Xiaoyong
    Mao, Dan
    Yang, Mei
    INORGANIC CHEMISTRY COMMUNICATIONS, 2010, 13 (07) : 831 - 833
12345