Synthesis and structure of a new three-dimentional open-framework zinc phosphate with 12-membered ring channels

被引：0

作者：

Wang, C ^{[1
]}

Li, J ^{[1
]}

Wang, Y ^{[1
]}

Wang, K ^{[1
]}

Yu, J ^{[1
]}

Xu, R ^{[1
]}

机构：

[1] Jilin Univ, State Key Lab Inorgan Synth & Preparat Chem, Changchun 130023, Peoples R China

来源：

RECENT ADVANCES IN THE SCIENCE AND TECHNOLOGY OF ZEOLITES AND RELATED MATERIALS, PTS A - C | 2004年 / 154卷

关键词：

zinc phosphate; open framework; hydrothermal synthesis; structure;

D O I：

暂无

中图分类号：

O64 [物理化学（理论化学）、化学物理学];

学科分类号：

070304 ; 081704 ;

摘要：

A new three-dimensional zinc phosphate [Zn6P5O20](3-)center dot[C6N3H15](3+)center dot H2O (I) has been hydrothermally synthesized from a reaction system Zn(OAC)(2)-1-(2-aminoethyl)piperazine-H3PO4-H2O. Single crystal X-ray diffraction analysis shows that it crystallizes in the monoclinic space group C2/c (no. 15) with a=20.240(4), b=16.856(3), c=8.1541(16)angstrom, beta=111.02(3)degrees, V=2596.7(9)angstrom(3) and Z=4. Its structure consists of one dimensional 12-membered ring channels along the [001] direction.

引用

页码：1035 / 1040

页数：6

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