Synthesis, spectroscopic characterization, and crystal structures of two chlorodiorganotin(IV) 4-(2-methoxyphenyl)piperazine-1-carbodithioates

被引：24

作者：

Zia-ur-Rehman ^{[1
,2
]}

Barsan, Mirela M. ^{[1
]}

Wharf, Ivor ^{[1
]}

Muhammad, Niaz ^{[2
]}

Ali, Saqib ^{[2
]}

Meetsma, Auke ^{[3
]}

Butler, Ian S. ^{[1
]}

机构：

[1] McGill Univ, Dept Chem, Montreal, PQ H3A 2K6, Canada

[2] Quaid I Azam Univ, Dept Chem, Islamabad 45320, Pakistan

[3] Univ Groningen, Crystal Struct Ctr, Zernike Inst Adv Mat, NL-9747 AG Groningen, Netherlands

来源：

INORGANICA CHIMICA ACTA | 2008年 / 361卷 / 11期

基金：

加拿大自然科学与工程研究理事会;

关键词：

Dithiocarboxylate; Chlorodiorganotin complexes; Raman; NMR; Mass spectra; X-ray diffraction;

D O I：

10.1016/j.ica.2008.05.006

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

Two chlorodiorganotin(IV) complexes of 4-(2-methoxyphenyl)piperazine-1-carbodithioate (MPPDA) have been synthesized by 1:1 mole-ratio reactions of the parent acid (MPPDAH) with Me2SnCl2 or Et2SnCl2 in dry methanol. The products have been characterized by Raman and multinuclear NMR (H-1, C-13 and Sn-119) spectroscopy, elemental analysis, and mass spectrometry. Single-crystal X-ray diffraction studies indicate that both complexes have distorted trigonal bipyramidal geometries around the central Sn atom. (C) 2008 Elsevier B.V. All rights reserved.

引用

页码：3322 / 3326

页数：5

共 50 条

[31] Synthesis, Crystal Structure and Biological Activity of N-(2-hydroxy-3-(4-(2-methoxyphenyl)-piperazin-1-yl)propyl)quinoxaline-2-methanamide
Huang Min-Yi
Xu Wei
Huang Jun-Jun
Huang Ya-Jian
Yuan Mu
CHINESE JOURNAL OF STRUCTURAL CHEMISTRY, 2015, 34 (04) : 497 - 502
[32] Synthesis and Crystal Structure of {η5:η1-[（2-Methoxyphenyl）-isopropyl]-indenyl}（dimethoxyethylene）lithium1
冯其琴
李一梅
王绍武
周双六
盛恩宏
黄子祥
Chinese Journal of Structural Chemistry, 2005, (09) : 1046 - 1048
[33] Synthesis, Crystal Structure and Biological Activity of N-(2-hydroxy-3-(4-(2-methoxyphenyl)-piperazin-1-yl)propyl)quinoxaline-2-methanamide
黄敏怡
徐未
黄珺珺
黄亚建
袁牧
结构化学, 2015, 34 (04) : 497 - 502
[34] Parallel synthesis and dopamine D3/D2 receptor screening of novel {4-[4-(2-methoxyphenyl)piperazin-1-yl]butyl}carboxamides
Heldler, P
Zohrabi-Kalantari, V
Calmels, T
Capet, M
Berrebi-Bertrand, I
Schwartz, JC
Stark, H
Link, A
BIOORGANIC & MEDICINAL CHEMISTRY, 2005, 13 (06) : 2009 - 2014
[35] Crystal and molecular structures of two triorganophosphinegold(I) 2-amino-cyclopent-1-ene-1-carbodithioates
Ho, SY
Tiekink, ERT
ZEITSCHRIFT FUR KRISTALLOGRAPHIE, 2004, 219 (08): : 513 - 518
[36] Synthesis, physicochemical characterization, DNA binding and in silico studies of (E)-4-((2-methoxyphenyl)amino)-4-oxobut-2-enoic acid and its triorganotin complexes
Sirajuddin, Muhammad
Ali, Saqib
Khan, Hizbullah
Tariq, Muhammad
JOURNAL OF CHEMICAL SCIENCES, 2022, 134 (02)
[37] 4-(4-Methoxyphenyl)-3-[2-(2-methoxyphenyl)ethyl]-1H-1,2,4-triazol-5(4H)-one
Hanif, Muhammad
Qadeer, Ghulam
Rama, Nasim Hasan
Akhtar, Javeed
Helliwell, Madeleine
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : O429 - U3073
[38] Synthesis, physicochemical characterization, DNA binding and in silico studies of (E)-4-((2-methoxyphenyl)amino)-4-oxobut-2-enoic acid and its triorganotin complexes
Muhammad Sirajuddin
Saqib Ali
Hizbullah Khan
Muhammad Tariq
Journal of Chemical Sciences, 2022, 134
[39] Synthesis, preclinical evaluation and molecular modelling of macrocyclic appended 1-(2-methoxyphenyl)piperazine for 5-HT1A neuroreceptor imaging
Hazari, Puja Panwar
Prakash, Surbhi
Meena, Virendra Kumar
Singh, Niraj
Chuttani, Krishna
Chadha, Nidhi
Singh, Pooja
Kukreti, Shrikant
Mishra, Anil Kumar
RSC ADVANCES, 2016, 6 (09) : 7288 - 7301
[40] 4-(2'-methoxyphenyl)-1-[2'-[N-(2''-pyridinyl)-p-iodobenzamido]ethyl]piperazine and 4-(2'-methoxyphenyl)-1-[2'-[N-(2''-pyridinyl)-p-fluorobenzamido]ethyl]piperazine, two new antagonists at pre- and postsynaptic serotonin-1A receptors
Thielen, RJ
Fangon, NB
Frazer, A
JOURNAL OF PHARMACOLOGY AND EXPERIMENTAL THERAPEUTICS, 1996, 277 (02): : 661 - 670

← 1 2 3 4 5 →