A new method to eliminate the influence of in situ contamination in SIMS analysis of hydrogen

被引:22
|
作者
Ludwig, Thomas
Stalder, Roland
机构
[1] Univ Heidelberg, Inst Mineral, D-69120 Heidelberg, Germany
[2] Univ Gottingen, Geowissensch Zent, Abt Mineral, D-37077 Gottingen, Germany
关键词
D O I
10.1039/b705848a
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
A new method has been developed that allows us to eliminate the influence of hydrogen contamination/background in SIMS analyses. The method is based on a number of measurements with different primary beam currents and a simple model for the sputtering of adsorbed hydrogen stemming from in situ contamination. Applying the contamination model to the data yields information about the degree of in situ contamination and about the relative intensity of H ions originating from the sample (e. g., H: Si ratio). The new method's advantage is that no other timeconsuming (such as special sample preparation and storage) or complicated and expensive (e. g., machine vacuum) measures to eliminate surface contamination are needed.
引用
收藏
页码:1415 / 1419
页数:5
相关论文
共 50 条
  • [41] SIMS studies of hydrogen interaction with the TiFe alloy surface: hydrogen influence on secondary ion yields
    Okseniuk, Ivan
    Shevchenko, Dmytro
    [J]. SURFACE SCIENCE, 2022, 716
  • [42] Cluster TOF-SIMS imaging:: A new light for in situ metabolomics?
    Mas, Sebastian
    Perez, Raul
    Martinez-Pinna, Roxana
    Egido, Jesus
    Vivanco, Fernando
    [J]. PROTEOMICS, 2008, 8 (18) : 3735 - 3745
  • [43] INFLUENCE OF PROBE CONTAMINATION ON RECOMBINATION OF ATOMIC-HYDROGEN
    COLLINS, LW
    DOWNS, WR
    [J]. COMBUSTION AND FLAME, 1975, 25 (02) : 277 - 278
  • [44] Using TOF-SIMS for the analysis of metal contamination on silicon wafers.
    Mowat, IA
    Schuerlein, T
    Metz, J
    Brigham, R
    Huffaker, D
    [J]. CLEANING TECHNOLOGY IN SEMICONDUCTOR DEVICE MANUFACTURING, 2000, 99 (36): : 561 - 568
  • [45] THE INFLUENCE OF HYDROGEN CONTAMINATION ON THE AMORPHIZATION REACTION OF CUTI ALLOYS
    IVISON, PK
    COWLAM, N
    SOLETTA, I
    COCCO, G
    ENCO, S
    BATTEZZATI, L
    [J]. MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING, 1991, 134 : 859 - 862
  • [46] Surface relaxation of Ti(0001): Influence of hydrogen contamination
    Teeter, G
    Erskine, JL
    [J]. PHYSICAL REVIEW B, 2000, 61 (20) : 13929 - 13935
  • [47] Analysis of amine contamination on silicon oxide surfaces using ToF-SIMS
    Lu, D
    Mo, ZQ
    Xing, ZX
    Gui, D
    [J]. APPLIED SURFACE SCIENCE, 2004, 233 (1-4) : 352 - 359
  • [48] DETECTION OF HYDROGEN IN METALS BY SIMS-METHOD WITH QUADRUPOLE MASS FILTER
    PAVLYAK, F
    BORI, L
    GIBER, J
    BUHL, R
    [J]. JAPANESE JOURNAL OF APPLIED PHYSICS, 1977, 16 (02) : 335 - 342
  • [49] SIMS analysis of low content hydrogen in commercially pure titanium
    Hamada, Shigeru
    Ohnishi, Katsu
    Nishikawa, Hide-aki
    Oda, Yasuji
    Noguchi, Hiroshi
    [J]. JOURNAL OF MATERIALS SCIENCE, 2009, 44 (20) : 5692 - 5696
  • [50] Matrix effects in hydrogen isotope analysis of silicate glasses by SIMS
    Hauri, Erik H.
    Shaw, Alison M.
    Wang, Jianhua
    Dixon, Jacqueline E.
    King, Penelope L.
    Mandeville, Charles
    [J]. CHEMICAL GEOLOGY, 2006, 235 (3-4) : 352 - 365