A new method to eliminate the influence of in situ contamination in SIMS analysis of hydrogen

被引:22
|
作者
Ludwig, Thomas
Stalder, Roland
机构
[1] Univ Heidelberg, Inst Mineral, D-69120 Heidelberg, Germany
[2] Univ Gottingen, Geowissensch Zent, Abt Mineral, D-37077 Gottingen, Germany
关键词
D O I
10.1039/b705848a
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
A new method has been developed that allows us to eliminate the influence of hydrogen contamination/background in SIMS analyses. The method is based on a number of measurements with different primary beam currents and a simple model for the sputtering of adsorbed hydrogen stemming from in situ contamination. Applying the contamination model to the data yields information about the degree of in situ contamination and about the relative intensity of H ions originating from the sample (e. g., H: Si ratio). The new method's advantage is that no other timeconsuming (such as special sample preparation and storage) or complicated and expensive (e. g., machine vacuum) measures to eliminate surface contamination are needed.
引用
收藏
页码:1415 / 1419
页数:5
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