Synthesis and Characterization of CdS Nanoparticles via Cyclic Microwave from Cadmium Oxalate

被引：5
|
作者：
Salavati-Niasari, Masoud [1 ,2 ]
Khoshroozi, Sanaz [1 ]
Sabet, Mohammad [3 ]
机构：
[1] Univ Kashan, Dept Inorgan Chem, Fac Chem, Kashan, Iran
[2] Univ Kashan, Inst Nano Sci & Nano Technol, Kashan, Iran
[3] Islamic Azad Univ, Sanandaj Branch, Dept Chem, Fac Sci, Sanandaj, Iran
来源：
JOURNAL OF CLUSTER SCIENCE | 2013年 / 24卷 / 01期
基金：
美国国家科学基金会;
关键词：
CdS; Nanoparticle; Cadmium oxalate; Microwave; SOLVOTHERMAL SYNTHESIS; HYDROTHERMAL PROCESS; NANOCRYSTALS; NANOSTRUCTURES; NANOFLOWERS; SULFIDE;
D O I：
10.1007/s10876-013-0556-5
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
The present study reports synthesis and characterization of CdS nanoparticles prepared by cyclic microwave route with the use of [Cd(C2O4)center dot 3H(2)O] powder as a precursor. The products, with an average size similar to 15 nm, were characterized by X-ray diffraction, scanning electron microscopy, energy dispersive X-ray microanalysis, thermogravimetric analysis, transmission electron microscopy and Fourier transform infrared spectroscopy. Optical property of obtained product was investigated by photoluminescence spectroscopy. The prepared nanostructures displayed a very strong luminescence at 528 nm (2.34 eV) at room temperature.
引用
收藏
页码：299 / 313
页数：15
相关论文
共 50 条
  • [21] Synthesis and characterization of zinc oxide nanoparticles via oxalate co-precipitation method
    Mahmood, Natheer B.
    Saeed, Farqad R.
    Gbashi, Kadhim R.
    Mahmood, Um-Salama
    MATERIALS LETTERS-X, 2022, 13
  • [22] Microwave synthesis and spectroscopic characterization of manganese oxalate nanocrystals
    Reddy, S. Lakshmi
    Reddy, G. Udayabashkar
    Reddy, R. Ramasubba
    Reddy, G. Siva
    Frost, Ray L.
    Endo, Tamio
    PARTICUOLOGY, 2013, 11 (03) : 340 - 345
  • [23] Microwave synthesis and spectroscopic characterization of manganese oxalate nanocrystals
    S.Lakshmi Reddy
    G.Udayabashkar Reddy
    R.Ramasubba Reddy
    G.Siva Reddy
    Ray L.Frostc
    Tamio Endo
    Particuology, 2013, 11 (03) : 340 - 345
  • [24] Synthesis of cadmium sulfide CdS nanoparticles in a silicate glass matrix
    Kuznetsova, Yu. V.
    Rempel, A. A.
    INORGANIC MATERIALS, 2015, 51 (09) : 933 - 938
  • [25] Synthesis of cadmium sulfide CdS nanoparticles in a silicate glass matrix
    Yu. V. Kuznetsova
    A. A. Rempel
    Inorganic Materials, 2015, 51 : 933 - 938
  • [26] Synthesis and characterization of cadmium selenide nanoparticles
    Coleman, Bridgett E.
    Lang, Patricia L.
    ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 2006, 231
  • [27] Microwave assisted synthesis of undoped and Cu doped CdS nanoparticles and their structural, morphological and optical characterization
    Tiwary, K. P.
    Sharma, K.
    Bala, Neha
    Ali, Firdaus
    MATERIALS TODAY-PROCEEDINGS, 2019, 18 : 1380 - 1387
  • [28] SYNTHESIS AND CHARACTERIZATION OF NICKEL DOPED CDs NANOPARTICLES
    Rao, B. Srinivasa
    Reddy, V. Rajagopal
    Kumar, B. Rajesh
    Rao, T. Subba
    INTERNATIONAL JOURNAL OF NANOSCIENCE, 2012, 11 (03)
  • [29] Synthesis and characterization of CdS nanoparticles modified with organic
    Yao, JX
    Zhao, GL
    Han, GR
    JOURNAL OF INORGANIC MATERIALS, 2003, 18 (02) : 445 - 450
  • [30] SYNTHESIS, STRUCTURAL AND OPTICAL CHARACTERIZATION OF CdS NANOPARTICLES
    Dwivedi, D. K.
    Dayashankar
    Dubey, Maheshwar
    JOURNAL OF OVONIC RESEARCH, 2010, 6 (01): : 57 - 62
12345