Synthesis and Characterization of CdS Nanoparticles via Cyclic Microwave from Cadmium Oxalate

被引：5

作者：

Salavati-Niasari, Masoud ^{[1
,2
]}

Khoshroozi, Sanaz ^{[1
]}

Sabet, Mohammad ^{[3
]}

机构：

[1] Univ Kashan, Dept Inorgan Chem, Fac Chem, Kashan, Iran

[2] Univ Kashan, Inst Nano Sci & Nano Technol, Kashan, Iran

[3] Islamic Azad Univ, Sanandaj Branch, Dept Chem, Fac Sci, Sanandaj, Iran

来源：

JOURNAL OF CLUSTER SCIENCE | 2013年 / 24卷 / 01期

基金：

美国国家科学基金会;

关键词：

CdS; Nanoparticle; Cadmium oxalate; Microwave; SOLVOTHERMAL SYNTHESIS; HYDROTHERMAL PROCESS; NANOCRYSTALS; NANOSTRUCTURES; NANOFLOWERS; SULFIDE;

D O I：

10.1007/s10876-013-0556-5

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

The present study reports synthesis and characterization of CdS nanoparticles prepared by cyclic microwave route with the use of [Cd(C2O4)center dot 3H(2)O] powder as a precursor. The products, with an average size similar to 15 nm, were characterized by X-ray diffraction, scanning electron microscopy, energy dispersive X-ray microanalysis, thermogravimetric analysis, transmission electron microscopy and Fourier transform infrared spectroscopy. Optical property of obtained product was investigated by photoluminescence spectroscopy. The prepared nanostructures displayed a very strong luminescence at 528 nm (2.34 eV) at room temperature.

引用

页码：299 / 313

页数：15

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