Synthesis and characterization of zinc oxide nanoparticles via oxalate co-precipitation method

被引：43
|
作者：
Mahmood, Natheer B. [1 ]
Saeed, Farqad R. [2 ]
Gbashi, Kadhim R. [3 ]
Mahmood, Um-Salama [4 ]
机构：
[1] Minist Educ, Gen Directorate Baghdad Educ Karkh2, Baghdad, Iraq
[2] Minist Sci & Technol, Directorate Mat Res, Baghdad, Iraq
[3] Univ Technol Baghdad, Nanotechnol & Adv Mat Res Ctr, Baghdad, Iraq
[4] Univ Baghdad, Al Khwarizmi Coll Engn, Baghdad, Iraq
来源：
MATERIALS LETTERS-X | 2022年 / 13卷
关键词：
ZnO nanopowder; Rietveld refinement; Oxalate co-precipitation method;
D O I：
10.1016/j.mlblux.2022.100126
中图分类号：
T [工业技术];
学科分类号：
08 ;
摘要：
Zinc Oxide nanoparticles (ZnO NPs) were synthesized as a powder using the oxalate co-precipitation method after calcination at 700 degrees C. Zine sulfate was used as a zinc soluble source, and oxalic acid was used as a Catalyst. The reaction was carried out at room temperature condition. The resulted powder was characterized by XRD analysis before calcination and after calcination at 500 degrees C, and 700 degrees C. The results show that the crystal structure is hexagonal with a = 3.249 angstrom, c = 5.205 angstrom. The FeSEM results showed particles of 80 nm.
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页数：4
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