Synthesis and Characterization of CdS Nanoparticles via Cyclic Microwave from Cadmium Oxalate

被引:5
|
作者
Salavati-Niasari, Masoud [1 ,2 ]
Khoshroozi, Sanaz [1 ]
Sabet, Mohammad [3 ]
机构
[1] Univ Kashan, Dept Inorgan Chem, Fac Chem, Kashan, Iran
[2] Univ Kashan, Inst Nano Sci & Nano Technol, Kashan, Iran
[3] Islamic Azad Univ, Sanandaj Branch, Dept Chem, Fac Sci, Sanandaj, Iran
基金
美国国家科学基金会;
关键词
CdS; Nanoparticle; Cadmium oxalate; Microwave; SOLVOTHERMAL SYNTHESIS; HYDROTHERMAL PROCESS; NANOCRYSTALS; NANOSTRUCTURES; NANOFLOWERS; SULFIDE;
D O I
10.1007/s10876-013-0556-5
中图分类号
O61 [无机化学];
学科分类号
070301 ; 081704 ;
摘要
The present study reports synthesis and characterization of CdS nanoparticles prepared by cyclic microwave route with the use of [Cd(C2O4)center dot 3H(2)O] powder as a precursor. The products, with an average size similar to 15 nm, were characterized by X-ray diffraction, scanning electron microscopy, energy dispersive X-ray microanalysis, thermogravimetric analysis, transmission electron microscopy and Fourier transform infrared spectroscopy. Optical property of obtained product was investigated by photoluminescence spectroscopy. The prepared nanostructures displayed a very strong luminescence at 528 nm (2.34 eV) at room temperature.
引用
收藏
页码:299 / 313
页数:15
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