Preparation and Characterization of PbS Nanoparticles via Cyclic Microwave Radiation Using Precursor of Lead (II) Oxalate

被引：20
|
作者：
Salavati-Niasari, Masoud [1 ,2 ]
Sobhani, Azam [3 ]
Khoshrooz, Sanaz [1 ]
Mirzanasiri, Noshin [4 ]
机构：
[1] Univ Kashan, Fac Chem, Dept Inorgan Chem, Kashan, Iran
[2] Univ Kashan, Inst Nano Sci & Nano Technol, Kashan, Iran
[3] Kosar Univ Bojnord, Dept Chem, Bojnord, Iran
[4] Univ Tehran, Coll Sci, Sch Chem, Tehran, Iran
来源：
JOURNAL OF CLUSTER SCIENCE | 2014年 / 25卷 / 04期
关键词：
Nanoparticles; PbS; Microwave; Lead (II) oxalate; Chemical synthesis; SOURCE MOLECULAR PRECURSOR; SONOCHEMICAL SYNTHESIS; HYDROTHERMAL SYNTHESIS; SINGLE; NANOCRYSTALS; NANOCUBES; MORPHOLOGY; CRYSTALS; NANORODS; GROWTH;
D O I：
10.1007/s10876-013-0674-0
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
PbS nanoparticles have been successfully synthesized through a simple, rapid microwave route using lead (II) oxalate as precursor, [Pb(O4C2)]. In this study, four different sulfur sources were applied that including sodium thiosulfate (Na2S2O3), thioacetamide (NH2CSCH3), thioglycolic acid (HSCH2CO2H), and l-cysteine (HO2CCH(NH2)CH2SH). The effects of sulfur sources on morphology and size of products in two different solvents, ethylene glycol (EG) and poly EG (PEG 400), were investigated. The products were analyzed by X-ray diffraction analysis, scanning electron microscopy, Fourier transform infrared spectroscopy and X-ray energy dispersive spectroscopy. Photoluminescence was used to study the optical properties of PbS nanoparticles.
引用
收藏
页码：937 / 947
页数：11
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