Quality assurance in accelerator mass spectrometry: Results from an international round-robin exercise for 10Be

The first international round-robin exercise for the measurement of the long-lived radionuclide Be-10 has been conducted. Ten participating accelerator mass spectrometry CAMS) facilities have each measured three samples at the 10(-12) to 10(-14) Be-10/Be-9 level. All results have been made traceable to the NISI SRM 4325 standard to avoid additional discrepancies that arise when different facilities use different calibration materials. Hence, the data concentrates on pure measurement distinctions. Multivariate statistical investigations have been performed to reveal a bias between facilities, i.e. two distinguished groups could be identified. Maximum discrepancies between two single facilities are in the range of 6-31% depending on the absolute Be-10/Be-9 value. These findings should be considered when comparing Be-10 data produced at one AMS facility with that produced at another facility, which is e.g. often the case for in situ Be-10 dating studies. Round-robin exercises are a very helpful tool as part of an overall quality assurance scheme to improve the accuracy, and not only the precision, of AMS data. (C) 2012 Elsevier B.V. All rights reserved.