Structural characterization of maleic anhydride grafted polyethylene by 13C NMR spectroscopy

被引：23

作者：

Yang, LQ ^{[1
]}

Zhang, FR ^{[1
]}

Endo, T ^{[1
]}

Hirotsu, T ^{[1
]}

机构：

[1] Natl Inst Adv Ind Sci & Technol, Inst Marine Resources & Environm Res, Takamatsu, Kagawa 7610395, Japan

来源：

POLYMER | 2002年 / 43卷 / 08期

关键词：

C-13 NMR spectroscopy; graft [2,3-C-13(2)] maleic anhydride;

D O I：

10.1016/S0032-3861(01)00802-3

中图分类号：

O63 [高分子化学（高聚物）];

学科分类号：

070305 ; 080501 ; 081704 ;

摘要：

Maleic anhydride grafted polyethylene, [2,3-C-13(2)] MA-g-PE, which was synthesized with C-13 labeled maleic anhydride [2,3-C-13(2)] MA in solution, was characterized by C-13 NMR spectroscopy in order to make clear the structure of graft groups. The results reveal that [2,3-C-13(2)] MA-g-PE has succinic anhydride oligomeric grafts with a terminal unsaturated MA ring in addition to well-known saturated succinic anhydride oligomeric grafts and that the former grafts are longer but fewer than the latter. (C) 2002 Elsevier Science Ltd. All rights reserved.

引用

页码：2591 / 2594

页数：4

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