Structural characterization of maleic anhydride grafted polyethylene by 13C NMR spectroscopy

被引：23
|
作者：
Yang, LQ [1 ]
Zhang, FR [1 ]
Endo, T [1 ]
Hirotsu, T [1 ]
机构：
[1] Natl Inst Adv Ind Sci & Technol, Inst Marine Resources & Environm Res, Takamatsu, Kagawa 7610395, Japan
来源：
POLYMER | 2002年 / 43卷 / 08期
关键词：
C-13 NMR spectroscopy; graft [2,3-C-13(2)] maleic anhydride;
D O I：
10.1016/S0032-3861(01)00802-3
中图分类号：
O63 [高分子化学（高聚物）];
学科分类号：
070305 ; 080501 ; 081704 ;
摘要：
Maleic anhydride grafted polyethylene, [2,3-C-13(2)] MA-g-PE, which was synthesized with C-13 labeled maleic anhydride [2,3-C-13(2)] MA in solution, was characterized by C-13 NMR spectroscopy in order to make clear the structure of graft groups. The results reveal that [2,3-C-13(2)] MA-g-PE has succinic anhydride oligomeric grafts with a terminal unsaturated MA ring in addition to well-known saturated succinic anhydride oligomeric grafts and that the former grafts are longer but fewer than the latter. (C) 2002 Elsevier Science Ltd. All rights reserved.
引用
收藏
页码：2591 / 2594
页数：4
相关论文
共 50 条
  • [31] Structural characterization of sulfur vulcanized deproteinized natural rubber by solid-state 13C NMR spectroscopy
    Sakdapipanich, JT
    Kowitteerawut, T
    Tuampoemsab, S
    Kawahara, S
    [J]. JOURNAL OF APPLIED POLYMER SCIENCE, 2006, 100 (03) : 1875 - 1880
  • [32] Synthesis of maleic anhydride grafted polyethylene and polypropylene, with controlled molecular structures
    Lu, B
    Chung, TC
    [J]. JOURNAL OF POLYMER SCIENCE PART A-POLYMER CHEMISTRY, 2000, 38 (08) : 1337 - 1343
  • [33] Space charge and electrical conduction in maleic anhydride-grafted polyethylene
    Lee, SH
    Park, JK
    Han, JH
    Suh, KS
    [J]. IEEE TRANSACTIONS ON DIELECTRICS AND ELECTRICAL INSULATION, 1995, 2 (06) : 1132 - 1139
  • [34] A study on extremely dilute/dilute solution of polyethylene grafted maleic anhydride
    Chen, ZJ
    Liu, ZX
    Xi, SP
    Gao, D
    Huang, Y
    [J]. ACTA POLYMERICA SINICA, 2000, (02) : 176 - 179
  • [35] High density polyethylene as a thermal storage material studied by MAS 13C NMR spectroscopy
    Han, OH
    Chae, SA
    Han, SO
    Woo, SK
    [J]. POLYMER, 1999, 40 (23) : 6329 - 6336
  • [36] Research progress of maleic anhydride grafted polyethylene for hot melt adhesive
    Li, Wen
    Zhang, Huahua
    Yan, Ruitao
    Zhou, Wenjuan
    Chen, Yanjun
    Zhang, Chaocan
    [J]. Huagong Jinzhan/Chemical Industry and Engineering Progress, 2016, 35 (09): : 2845 - 2849
  • [37] Structural study of four Ca@C82 isomers by 13C NMR spectroscopy
    Kodama, T
    Fujii, R
    Miyake, Y
    Sakaguchi, K
    Nishikawa, H
    Ikemoto, I
    Kikuchi, K
    Achiba, Y
    [J]. CHEMICAL PHYSICS LETTERS, 2003, 377 (1-2) : 197 - 200
  • [38] Structural study of three isomers of Tm@C82 by 13C NMR spectroscopy
    Kodama, T
    Ozawa, N
    Miyake, Y
    Sakaguchi, K
    Nishikawa, H
    Ikemoto, I
    Kikuchi, K
    Achiba, Y
    [J]. JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 2002, 124 (07) : 1452 - 1455
  • [39] 13C NMR STUDY OF THE STRUCTURE OF POLYETHYLENE-POLYAMINES.
    Bulai, A.Kh.
    Slonim, I.Ya.
    Urman, Ya.G.
    Vakulenko, V.A.
    Chetverikova, A.T.
    [J]. Polymer science USSR, 1986, 28 (08): : 1854 - 1858
  • [40] Quantitative 13C NMR Spectroscopy of Humic Acids
    Novak, Frantisek
    Hrabal, Richard
    [J]. CHEMICKE LISTY, 2011, 105 (10): : 752 - 760
12345