ONE STEP PROTOCOL AND GREEN SYNTHESIS OF 2-N,N-DIMETHYLAMINO-3-ALKYL(ARYL)-2-OXIDO-1-HYDRO-2-BENZO[1,3,2]DIAZAPHOSPHININE-4-ONE DERIVATIVES

被引：1

作者：

Amor, A. Ben Hadj ^{[1
]}

Abderrahim, R. ^{[1
]}

机构：

[1] Univ Carthage, Fac Sci Bizerte, LR Ressource Materiaux & Ecosyst, Mat Lamellaires & Nanomat Hybrides, Bizerte 7021, Tunisia

来源：

BULLETIN OF THE CHEMICAL SOCIETY OF ETHIOPIA | 2022年 / 36卷 / 04期

关键词：

Anthranilic acid; N; N-Dimethylphosphoramic dichloride; Diazaphosphinine; 2-OXIDES;

D O I：

10.4314/bcse.v36i4.11

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

2-N,N-dimethylamino-2-oxido-3-alkyl(aryl)-1-hydro-2-b enzo[1,3,2]diazaphosphinin-4-one (2) derivatives are synthesized by one pot reaction by reacting equimolar quantities of anthranilic acid, primary amine, and N,N-dimethylphosphoramic dichloride under reflux of ethanol with good yields. The structure of the compounds were established on the basis of their infrared, nuclear magnetic resonance spectral data (H-1 NMR, C-13 NMR and 31P NMR), mass spectrometry, and elemental analysis.

引用

页码：859 / 864

页数：6

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