ONE STEP PROTOCOL AND GREEN SYNTHESIS OF 2-N,N-DIMETHYLAMINO-3-ALKYL(ARYL)-2-OXIDO-1-HYDRO-2-BENZO[1,3,2]DIAZAPHOSPHININE-4-ONE DERIVATIVES

被引：1
|
作者：
Amor, A. Ben Hadj [1 ]
Abderrahim, R. [1 ]
机构：
[1] Univ Carthage, Fac Sci Bizerte, LR Ressource Materiaux & Ecosyst, Mat Lamellaires & Nanomat Hybrides, Bizerte 7021, Tunisia
来源：
BULLETIN OF THE CHEMICAL SOCIETY OF ETHIOPIA | 2022年 / 36卷 / 04期
关键词：
Anthranilic acid; N; N-Dimethylphosphoramic dichloride; Diazaphosphinine; 2-OXIDES;
D O I：
10.4314/bcse.v36i4.11
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
2-N,N-dimethylamino-2-oxido-3-alkyl(aryl)-1-hydro-2-b enzo[1,3,2]diazaphosphinin-4-one (2) derivatives are synthesized by one pot reaction by reacting equimolar quantities of anthranilic acid, primary amine, and N,N-dimethylphosphoramic dichloride under reflux of ethanol with good yields. The structure of the compounds were established on the basis of their infrared, nuclear magnetic resonance spectral data (H-1 NMR, C-13 NMR and 31P NMR), mass spectrometry, and elemental analysis.
引用
收藏
页码：859 / 864
页数：6
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