Reaction of 4,6-Di-tert-butyl-3-nitrocyclohexa-3,5-diene-1,2-dione with Secondary Amines

被引：0
|
作者：
Ivakhnenko, E. P. [1 ]
Malai, V. I. [1 ]
Demidov, O. P. [2 ]
Minkin, V. I. [1 ]
机构：
[1] Southern Fed Univ, Inst Phys & Organ Chem, Rostov Na Donu 344090, Russia
[2] North Caucasus Fed Univ, Stavropol 355029, Russia
来源：
RUSSIAN JOURNAL OF ORGANIC CHEMISTRY | 2023年 / 59卷 / 08期
基金：
俄罗斯科学基金会;
关键词：
nitroquinone; o-quinone; secondary amines; ANRORC; Michael addition; PRODUCTS;
D O I：
10.1134/S1070428023080043
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
The reaction of 4,6-di-tert-butyl-3-nitrocyclohexa-3,5-diene-1,2-dione with secondary amines (piperidine, morpholine, 1-methylpiperazine) in isopropanol involves Michael addition and ANRORC and forms a mixture of products. The resulting compounds were characterized by IR and H-1 and C-13 NMR spectroscopy, and elemental analysis. The molecular structures of 3-nitrocyclohexa-3-ene-1,2-dione and cyclopenta-1,3-diene derivatives were established by X-ray diffraction analysis.
引用
收藏
页码：1315 / 1321
页数：7
相关论文
共 50 条
  • [41] Synthesis and properties of phosphorylated of 3,5-Di-tert-butyl-4-hydroxybenzylhydrazines
    Ismagilov, RK
    Moskva, VV
    Mosunova, LY
    Arkhipov, VP
    RUSSIAN JOURNAL OF GENERAL CHEMISTRY, 2000, 70 (01) : 46 - 47
  • [42] Reactions of 3,5-di-tert-butyl-1,2-benzoquinone with mercapto carboxylic acids
    Ukhin, L. Yu.
    Suponitsky, K. Yu.
    Shepelenko, E. N.
    Belousova, L. V.
    Alekseenko, D. V.
    Borodkin, G. S.
    Etmetchenko, L. N.
    RUSSIAN CHEMICAL BULLETIN, 2016, 65 (03) : 727 - 730
  • [43] Interaction of 3,5-di-tert-butyl-4-hydroxybenzylacetate with malonic ester
    Bukharov, SV
    Nugumanova, GN
    Mukmeneva, NA
    ZHURNAL OBSHCHEI KHIMII, 1999, 69 (04): : 699 - 699
  • [44] Oxidative rearrangement of 3,5-di-tert-butyl-4-hydroxybenzaldehyde acetals
    Pugovics, O
    Kauss, V
    Kalvinsh, I
    Gold, MR
    JOURNAL OF CHEMICAL RESEARCH, 1998, (08) : 470 - 471
  • [45] ANTIOXIDANT ACTIVITY OF 3,5-DI-TERT-BUTYL-4-HYDROXYBENZYL DERIVATIVES
    KIM, DH
    KUMMEROW, FA
    JOURNAL OF THE AMERICAN OIL CHEMISTS SOCIETY, 1962, 39 (03) : 150 - &
  • [46] The reaction of 3,6-di-tert-butyl-1,2-benzoquinone and 3,6-di-tert-butylcatechol withtert-butyl hydroperoxide
    V. N. Glushakova
    N. A. Skorodumova
    V. I. Nevodchikov
    L. G. Abakumova
    N. P. Makarenko
    V. K. Cherkasov
    N. O. Druzhkov
    Russian Chemical Bulletin, 1999, 48 : 934 - 937
  • [47] SYNTHESIS OF TRIS(3,5-DI-TERT-BUTYL-4-HYDROXYBENZYL)-PHOSPHINE
    MUKMENEVA, NA
    KADYROVA, VK
    CHEREZOVA, EN
    SHARIFULLIN, AS
    ZHURNAL OBSHCHEI KHIMII, 1993, 63 (08): : 1909 - 1910
  • [48] SYNTHESIS OF DIALKYL(3,5-DI-TERT-BUTYL-4-HYDROXYPHENYL)-PHOSPHATES
    MUKHMENEVA, NA
    KADYROVA, VK
    MOSKVA, VV
    MOSKVA, NA
    ZHURNAL OBSHCHEI KHIMII, 1985, 55 (03): : 696 - 697
  • [49] N-(3,5-di-tert-butyl-4-hydroxybenzyl)phthalimide
    Xin, CW
    Li, JS
    Guo, ZX
    Chen, LG
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2006, 62 : O1273 - O1275
  • [50] DIETHYLPHOSPHONATE AND TRIETHYLPHOSPHITE INTERACTION WITH 3,5-DI-TERT-BUTYL-4-HYDROXYBENZALDEHYDE
    ISMAGILOV, RK
    MOSKVA, VV
    BAGAUTDINOVA, DB
    ARKHIPOV, VP
    KOPYLOVA, LY
    ZHURNAL OBSHCHEI KHIMII, 1992, 62 (11): : 2488 - 2491
12345