Reaction of 4,6-Di-tert-butyl-3-nitrocyclohexa-3,5-diene-1,2-dione with Secondary Amines

被引：0
|
作者：
Ivakhnenko, E. P. [1 ]
Malai, V. I. [1 ]
Demidov, O. P. [2 ]
Minkin, V. I. [1 ]
机构：
[1] Southern Fed Univ, Inst Phys & Organ Chem, Rostov Na Donu 344090, Russia
[2] North Caucasus Fed Univ, Stavropol 355029, Russia
来源：
RUSSIAN JOURNAL OF ORGANIC CHEMISTRY | 2023年 / 59卷 / 08期
基金：
俄罗斯科学基金会;
关键词：
nitroquinone; o-quinone; secondary amines; ANRORC; Michael addition; PRODUCTS;
D O I：
10.1134/S1070428023080043
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
The reaction of 4,6-di-tert-butyl-3-nitrocyclohexa-3,5-diene-1,2-dione with secondary amines (piperidine, morpholine, 1-methylpiperazine) in isopropanol involves Michael addition and ANRORC and forms a mixture of products. The resulting compounds were characterized by IR and H-1 and C-13 NMR spectroscopy, and elemental analysis. The molecular structures of 3-nitrocyclohexa-3-ene-1,2-dione and cyclopenta-1,3-diene derivatives were established by X-ray diffraction analysis.
引用
收藏
页码：1315 / 1321
页数：7
相关论文
共 50 条
  • [21] INTERACTION OF 3,5-DI-TERT-BUTYL-4-HYDROXYBENZYLACETATE WITH TRIALKYLPHOSPHITES
    MUKMENEVA, NA
    CHEREZOVA, EN
    ZHUKOVA, RS
    ZHURNAL OBSHCHEI KHIMII, 1994, 64 (06): : 1049 - 1049
  • [22] 3,5-di-tert-butyl-1,2-benzoquinone as model substance of pyridoxal
    Vinsová, J
    Horák, V
    CHEMICKE LISTY, 2003, 97 (12): : 1157 - 1167
  • [23] CYCLIC ACETALS OF 3,5-DI-TERT-BUTYL-4-HYDROXYBENZALDEHYDE
    SKURKO, MR
    ZLOTSKII, SS
    BELOV, PS
    RAKHMANKULOV, DL
    KARAKHANOV, RA
    JOURNAL OF APPLIED CHEMISTRY OF THE USSR, 1979, 52 (01): : 211 - 214
  • [24] Certain reactions of 3,5-di-tert-butyl-4-hydroxybenzylacetate
    Mukmeneva, NA
    Kadyrova, VK
    Bukharov, SV
    Nugumanova, GN
    ZHURNAL OBSHCHEI KHIMII, 1996, 66 (10): : 1725 - 1727
  • [25] 3-(3,5-Di-tert-butyl-4-hydroxyphenyl)-propionohydrazide
    Xu, WM
    Hu, XR
    Gu, JM
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2005, 61 : O4190 - O4191
  • [26] Reaction of 8-arenesulfonyloxy-2-methylquinolines with 4,6-di(tert-butyl)-3-nitro-1,2-benzoquinone
    Mikhailov, I. E.
    Kolodina, A. A.
    Artyushkina, Yu. M.
    Dushenko, G. A.
    Sayapin, Yu. A.
    Minkin, V. I.
    RUSSIAN JOURNAL OF ORGANIC CHEMISTRY, 2015, 51 (04) : 595 - 598
  • [27] Reaction of 8-arenesulfonyloxy-2-methylquinolines with 4,6-di(tert-butyl)-3-nitro-1,2-benzoquinone
    I. E. Mikhailov
    A. A. Kolodina
    Yu. M. Artyushkina
    G. A. Dushenko
    Yu. A. Sayapin
    V. I. Minkin
    Russian Journal of Organic Chemistry, 2015, 51 : 595 - 598
  • [28] SCREENED PHENOLS .3. STABILIZATION OF POLYOLEFINS BY 3,5-DI-TERT-BUTYL-4-HYDROXYBENZYLIDENEAMINES AND N-SUBSTITUTED 3,5-DI-TERT-BUTYL-4-HYDROXYBENZYLAMINES
    BRUK, YA
    ZOLOTOVA, LV
    BORODULINA, MZ
    JOURNAL OF APPLIED CHEMISTRY OF THE USSR, 1976, 48 (12): : 2815 - 2818
  • [29] Reaction of 3,5-Di-tert-butyl-4-hydroxybenzylidene Chloride with P(III) Acid Esters
    M. B. Gazizov
    R. K. Ismagilov
    L. M. Shamsutdinova
    R. F. Karimova
    O. G. Sinyashin
    Russian Journal of General Chemistry, 2005, 75 : 1971 - 1972
  • [30] New data on the reaction of diethyl hydrogen phosphite with 3,5-di-tert-butyl-4-hydroxybenzaldehyde
    Ismagilov, RK
    Moskva, VV
    Mosunova, LY
    Romakhin, AS
    RUSSIAN JOURNAL OF GENERAL CHEMISTRY, 2001, 71 (10) : 1547 - 1549
12345