5-Anilino-3-benzylsulfanyl-6-(3-chloroanilino)-1-phenyl-1H-pyrazolo[3,4-d]pyrimidin-4(5H)-one

被引：0

作者：

Wang, Hong-Qing ^{[1
]}

He, Fang-Fang ^{[1
]}

Wang, Xiao-Feng ^{[1
]}

Zhou, Wei-Ping ^{[2
]}

Liu, Zhao-Jie ^{[3
]}

机构：

[1] Univ South China, Sch Chem & Chem Engn, Hengyang 421001, Peoples R China

[2] Univ South China, Coll Math & Phys, Hunan 421001, Peoples R China

[3] Cent China Normal Univ, Inst Organ Synth, Wuhan 430079, Hubei, Peoples R China

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2012年 / 68卷

基金：

美国国家科学基金会;

关键词：

D O I：

10.1107/S1600536812037683

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

In the title compound, C30H23ClN6OS, the benzyl, the 3chloroanilino, the phenyl and the anilino groups form dihedral angles of 85.95 (6), 29.63 (7), 28.55 (1) and 87.48 (6)degrees, respectively, with the pyrazolo[3,4-d] pyrimidine unit [maximum deviation = 0.052 (2) angstrom]. An intramolecular NH center dot center dot center dot N hydrogen bond occurs. The crystal structure features N-H center dot center dot center dot O hydrogen bonds.

引用

页码：O2895 / +

页数：10

共 50 条

[41] Ethyl (4-oxo-1-phenyl-1,4-dihydro-5H-pyrazolo[3,4-d]pyrimidin-5-yl) acetate
Yathirajan, H. S.
Bindya, S.
Sarojini, B. K.
Narayana, B.
Bolte, Michael
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2007, 63 : O2718 - U1533
[42] Catalytic synthesis of 6-aryl-1H-pyrazolo[3,4-d]pyrimidin-4[5H]-ones by heteropolyacid:: H14[NaP5W30O110] and H3PW12O40
Heravi, MM
Motamedi, R
Seifi, N
Bamoharram, FF
JOURNAL OF MOLECULAR CATALYSIS A-CHEMICAL, 2006, 249 (1-2) : 1 - 3
[43] Design and Synthesis of Novel Thioethers Derived from 1,5-Diphenyl-6-thioxo-6,7-dihydro-1H-pyrazolo[3,4-d]pyrimidin-4(5H)-ones as Antiangiogenic Agents
Malki, Ahmed
Issa, Doaa A. E.
Elbayaa, Rasha Y.
Ashour, Hayam M. A.
LETTERS IN DRUG DESIGN & DISCOVERY, 2019, 16 (02) : 200 - 212
[44] Methyl (4-oxo-1-phenyl-4,5-dihydro-1H-pyrazolo[3,4-d] pyrimidin-5-yl)acetate
Yathirajan, H. S.
Bindya, S.
Sarojini, B. K.
Narayana, B.
Bolte, Michael
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2007, 63 : O2566 - U1040
[45] The crystal structure of 1,5-dibenzyl-1H-pyrazolo[3,4-d]pyrimidine-4(5H)-thione
El Fal, Mohammed
Ramli, Youssef
Essassi, El Mokhtar
Saadi, Mohamed
El Ammari, Lahcen
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2015, 71 : O95 - U406
[46] 4-(3-Phenyl-1H-pyrazolo[3,4-d]pyrimidin-1-yl)thieno[3,2-d]pyrimidine
Noh, Eun Sun
Kim, Sung Min
Song, Yang-Heon
MOLBANK, 2020, 2020 (02)
[47] A catalytic method for synthesis of 6-aryl-1H-pyrazolo[3,4-d]pyrimidin-4[5H]-ones by heteropolyacids:: H14[NaP5W29MoO110] and H3PMo12O40
Heravi, Majid M.
Motamedi, Radineh
Bamoharram, Fatemeh F.
Seify, Nasim
CATALYSIS COMMUNICATIONS, 2007, 8 (10) : 1467 - 1471
[48] THE SYNTHESIS OF PYRAZOLO[3,4-D]PYRIDAZINES - PHOTOCHEMICAL CYCLIZATION TO "PYRAZOLO[3,4-D]PYRIDAZIN-4(5H)-ONES WITH SUBSEQUENT FUNCTIONALIZATION
KAJI, K
NAGASHIMA, H
OHTA, Y
TABASHI, K
ODA, H
JOURNAL OF HETEROCYCLIC CHEMISTRY, 1984, 21 (05) : 1249 - 1255
[49] STRUCTURE OF 1,5,6-TRIMETHYL-1H-PYRAZOLO[3,4-D]PYRIDAZINE-4,7(5H,6H)-DIONE
LEBAN, I
GOLIC, L
STANOVNIK, B
TISLER, M
ACTA CRYSTALLOGRAPHICA SECTION C-STRUCTURAL CHEMISTRY, 1988, 44 : 193 - 195
[50] STUDIES ON PYRAZOLO[3,4-D]PYRIMIDINE DERIVATIVES .5. TRANSFORMATION OF PYRAZOLO[3,4-D]PYRIMIDINES-H-1 INTO PYRAZOLO[3,4-B]PYRIDINES-H-1
HIGASHINO, T
IWAI, Y
HAYASHI, E
CHEMICAL & PHARMACEUTICAL BULLETIN, 1977, 25 (04) : 535 - 542

← 1 2 3 4 5 →