5-Anilino-3-benzylsulfanyl-6-(3-chloroanilino)-1-phenyl-1H-pyrazolo[3,4-d]pyrimidin-4(5H)-one

被引：0

作者：

Wang, Hong-Qing ^{[1
]}

He, Fang-Fang ^{[1
]}

Wang, Xiao-Feng ^{[1
]}

Zhou, Wei-Ping ^{[2
]}

Liu, Zhao-Jie ^{[3
]}

机构：

[1] Univ South China, Sch Chem & Chem Engn, Hengyang 421001, Peoples R China

[2] Univ South China, Coll Math & Phys, Hunan 421001, Peoples R China

[3] Cent China Normal Univ, Inst Organ Synth, Wuhan 430079, Hubei, Peoples R China

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2012年 / 68卷

基金：

美国国家科学基金会;

关键词：

D O I：

10.1107/S1600536812037683

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

In the title compound, C30H23ClN6OS, the benzyl, the 3chloroanilino, the phenyl and the anilino groups form dihedral angles of 85.95 (6), 29.63 (7), 28.55 (1) and 87.48 (6)degrees, respectively, with the pyrazolo[3,4-d] pyrimidine unit [maximum deviation = 0.052 (2) angstrom]. An intramolecular NH center dot center dot center dot N hydrogen bond occurs. The crystal structure features N-H center dot center dot center dot O hydrogen bonds.

引用

页码：O2895 / +

页数：10

共 50 条

[31] SYNTHESIS OF PYRAZOLO[3,4-D]PYRIDAZINES - THIONATION FOLLOWED BY ALKYLATION OF PYRAZOLO[3,4-D]PYRIDAZIN-4(5H)-ONE
KAJI, K
NAGASHIMA, H
TABASHI, K
ODA, H
HETEROCYCLES, 1984, 22 (10) : 2357 - 2362
[32] Novel 1,5-diphenyl-6-substituted 1H-pyrazolo[3,4-d]pyrimidin-4(5H)-ones induced apoptosis in RKO colon cancer cells
Malki, Ahmed
Ashour, Hayam M. A.
Elbayaa, Rasha Y.
Issa, Doaa A. E.
Aziz, Hassan A.
Chen, Xiaozhuo
JOURNAL OF ENZYME INHIBITION AND MEDICINAL CHEMISTRY, 2016, 31 (06) : 1286 - 1299
[33] STUDIES ON PYRAZOLO[3,4-D]PYRIMIDINE DERIVATIVES .9. 4-(P-TOLYLSULFONYL)-1-PHENYL-1H-PYRAZOLO[3,4-D]PYRIMIDINE
HAYASHI, E
HIGASHINO, T
SUZUKI, SI
YAKUGAKU ZASSHI-JOURNAL OF THE PHARMACEUTICAL SOCIETY OF JAPAN, 1978, 98 (01): : 89 - 94
[34] SYNTHESIS OF THE BETA-D-DEOXYRIBOFURANOSIDE OF 6-AMINO-H-1-PYRAZOLO [3,4-D]-PYRIMIDIN-4(H-5)-ONE - A NEW ISOSTER OF 2'-DEOXYGUANOSINE
SEELA, F
STEKER, H
HETEROCYCLES, 1985, 23 (10) : 2521 - 2524
[35] Synthesis of pyrazolo[3,4-d]pyrimidin-4(5H)-ones tethered to 1,2,3-triazoles and their evaluation as potential anticancer agents
Allam, Muralidhar
Bhavani, A. K. D.
Mudiraj, Anwita
Ranjan, Nikhil
Thippana, Mallikarjuna
Babu, Phanithi Prakash
EUROPEAN JOURNAL OF MEDICINAL CHEMISTRY, 2018, 156 : 43 - 52
[36] Acidic cesium salt of Preyssler nanoparticles: a new, green and recyclable nanocatalyst for the synthesis of 6-aryl-1H-pyrazolo[3,4-d]pyrimidin-4[5H]-ones
Bamoharram F.F.
Heravi M.M.
Ayati A.
Baharara J.
Jafari A.M.
Ebrahimi M.
Journal of Nanostructure in Chemistry, 2014, 4 (2)
[37] SYNTHESIS OF 6-AMINO-1-(BETA-D-RIBOFURANOSYL)-1H-PYRAZOLO[3,4-D]-1,3-OXAZIN-4-ONE, AN ISOSTERE OF OXANOSINE, AND THE GUANOSINE ANALOG 6-AMINO-1-(BETA-D-RIBOFURANOSYL)-1H-PYRAZOLO[3,4-D]PYRIMIDIN-4(5H)-ONE VIA RING-CLOSURE OF PYRAZOLE-5-THIOUREIDO INTERMEDIATES
BHATTACHARYA, BK
ROBINS, RK
REVANKAR, GR
JOURNAL OF HETEROCYCLIC CHEMISTRY, 1990, 27 (03) : 787 - 793
[38] Synthesis of novel isoxazolines and isoxazoles of N-substituted pyrazolo[3,4-d]pyrimidin-4(5H)-one derivatives through [3+2] cycloaddition
Rahmouni, Ameur
Romdhane, Anis
Ben Said, Abderrahim
Guerineau, Vincent
Touboul, David
Ben Jannet, Hichem
ARABIAN JOURNAL OF CHEMISTRY, 2019, 12 (08) : 1974 - 1982
[39] STUDIES ON PYRAZOLO[3,4-D]PYRIMIDINE DERIVATIVES .10. REACTION OF 1-PHENYL-1H-PYRAZOLO[3,4-D]PYRIMIDINE 5-OXIDE WITH METHANESULFONYL CHLORIDE AND POTASSIUM CYANIDE
HAYASHI, E
HIGASHINO, T
SHIMADA, N
YAKUGAKU ZASSHI-JOURNAL OF THE PHARMACEUTICAL SOCIETY OF JAPAN, 1978, 98 (02): : 234 - 235
[40] Synthesis of novel 1,2-(un) substituted-3-amino-5-aryl-6-arylaminopyrazolo[3,4-d]pyrimidin-4(5H)-ones and their biological activities
Shishoo, CJ
Ravikumar, T
Jain, KS
Rathod, IS
Gandhi, TP
Satia, MC
INDIAN JOURNAL OF CHEMISTRY SECTION B-ORGANIC CHEMISTRY INCLUDING MEDICINAL CHEMISTRY, 1999, 38 (09): : 1075 - 1085

← 1 2 3 4 5 →