5-Anilino-3-benzylsulfanyl-6-(3-chloroanilino)-1-phenyl-1H-pyrazolo[3,4-d]pyrimidin-4(5H)-one

被引：0
|
作者：
Wang, Hong-Qing [1 ]
He, Fang-Fang [1 ]
Wang, Xiao-Feng [1 ]
Zhou, Wei-Ping [2 ]
Liu, Zhao-Jie [3 ]
机构：
[1] Univ South China, Sch Chem & Chem Engn, Hengyang 421001, Peoples R China
[2] Univ South China, Coll Math & Phys, Hunan 421001, Peoples R China
[3] Cent China Normal Univ, Inst Organ Synth, Wuhan 430079, Hubei, Peoples R China
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2012年 / 68卷
基金：
美国国家科学基金会;
关键词：
D O I：
10.1107/S1600536812037683
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
In the title compound, C30H23ClN6OS, the benzyl, the 3chloroanilino, the phenyl and the anilino groups form dihedral angles of 85.95 (6), 29.63 (7), 28.55 (1) and 87.48 (6)degrees, respectively, with the pyrazolo[3,4-d] pyrimidine unit [maximum deviation = 0.052 (2) angstrom]. An intramolecular NH center dot center dot center dot N hydrogen bond occurs. The crystal structure features N-H center dot center dot center dot O hydrogen bonds.
引用
收藏
页码：O2895 / +
页数：10
相关论文
共 50 条
  • [21] 4-Benzylsulfanyl-1H-pyrazolo[3,4-d]pyrimidine
    El Fal, Mohammed
    Ramli, Youssef
    Essassi, El Mokhtar
    Saadi, Mohamed
    El Ammari, Lahcen
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2013, 69 : O1650 - +
  • [22] Electrophilic Heterocyclization of 6-Alken(yn)ylsulfanyl-pyrazolo[3,4-d]pyrimidin-4(5H)-ones
    Bentya, A. V.
    Vas'kevich, R. I.
    Bol'but, A. V.
    Vovk, M. V.
    Staninets, V. I.
    Turov, A. V.
    Rusanov, E. B.
    RUSSIAN JOURNAL OF ORGANIC CHEMISTRY, 2008, 44 (09) : 1362 - 1368
  • [23] (3,5-Dimethylpyrazol-1-yl)-[4-(1-phenyl-1H-pyrazolo[3,4-d]pyrimidin-4-ylamino)phenyl] methanone
    Bakr, Rania B.
    Mehany, Ahmed B. M.
    MOLBANK, 2016, (04)
  • [24] Cyclofunctionalization of 6-alkenylsulfanylpyrazolo[3,4-d]-pyrimidin-4(5H)-ones with arenesulfenyl chlorides
    Vas'kevich, A. I.
    Bentya, A. V.
    Staninets, V. I.
    RUSSIAN JOURNAL OF ORGANIC CHEMISTRY, 2009, 45 (12) : 1847 - 1852
  • [25] Cyclofunctionalization of 6-alkenylsulfanylpyrazolo[3,4-d]-pyrimidin-4(5H)-ones with arenesulfenyl chlorides
    A. I. Vas’kevich
    A. V. Bentya
    V. I. Staninets
    Russian Journal of Organic Chemistry, 2009, 45 : 1847 - 1852
  • [26] STUDIES ON PYRAZOLO[3,4-D]PYRIMIDINE DERIVATIVES .11. 1-PHENYL-1H-PYRAZOLO[3,4-D]PYRIMIDINE-4-CARBONITRILE
    HAYASHI, E
    HIGASHINO, T
    SUZUKI, S
    YAKUGAKU ZASSHI-JOURNAL OF THE PHARMACEUTICAL SOCIETY OF JAPAN, 1978, 98 (07): : 891 - 897
  • [27] 4-AMINO-1-PHENYLPYRAZOLO[3,4-D]PYRIMIDIN-6(5H)-ONE, AN ISOGUANOSINE ANALOG
    QUINN, RJ
    SCAMMELLS, PJ
    AUSTRALIAN JOURNAL OF CHEMISTRY, 1991, 44 (07) : 1001 - 1005
  • [28] Synthesis of new imidazo[1,2-a]pyrazolo[4,3-e]pyrimidin-4(6H)-one derivatives by iodocyclization of 6-alkenyl(alkynyl)-aminopyrazolo[3,4-d]pyrimidin-4(5H)-ones
    A. V. Bentya
    R. I. Vas’kevich
    A. V. Turov
    E. B. Rusanov
    M. V. Vovk
    V. I. Staninets
    Russian Journal of Organic Chemistry, 2011, 47 : 1066 - 1073
  • [29] Synthesis of new imidazo[1,2-a]pyrazolo[4,3-e]pyrimidin-4(6H)-one derivatives by iodocyclization of 6-alkenyl(alkynyl)-aminopyrazolo[3,4-d]pyrimidin-4(5H)-ones
    Bentya, A. V.
    Vas'kevich, R. I.
    Turov, A. V.
    Rusanov, E. B.
    Vovk, M. V.
    Staninets, V. I.
    RUSSIAN JOURNAL OF ORGANIC CHEMISTRY, 2011, 47 (07) : 1066 - 1073
  • [30] SYNTHESIS AND INVITRO ANTIFUNGAL ACTIVITY OF 6-TRIFLUOROMETHYLPYRAZOLO[3,4-D]PYRIMIDIN-4(5H)-THIONES
    VICENTINI, CB
    POLI, T
    VERONESE, AC
    BRANDOLINI, V
    MANFRINI, M
    GUARNERI, M
    GIORI, P
    PESTICIDE SCIENCE, 1989, 27 (01): : 77 - 83
12345