STRUCTURE OF 2,2,4,4-TETRAKIS(TRIFLUOROMETHYL)-1,3-DISELENETANE

被引:7
|
作者
RABE, G [1 ]
KELLER, K [1 ]
ROESKY, HW [1 ]
LAGOW, RJ [1 ]
PAUER, F [1 ]
STALKE, D [1 ]
机构
[1] UNIV GOTTINGEN,INST ANORGAN CHEM,TAMMANNSTR 4,W-3400 GOTTINGEN,GERMANY
关键词
HEXAFLUOROSELENOACETONE; X-RAY;
D O I
10.1515/znb-1991-0205
中图分类号
O61 [无机化学];
学科分类号
070301 ; 081704 ;
摘要
The reaction of hexafluoroacetone with triphenylphosphane selenide proceeds with elimination of triphenylphosphate oxide to yield 2,2,4,4-tetrakis(trifluormethyl)-1,3-diselenetane (1). Crystals of 1 that are suitable for X-ray crystal structure analysis have been obtained by recrystallization from hexane.
引用
收藏
页码:157 / 160
页数:4
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