STRUCTURE OF 2,2,4,4-TETRAKIS(TRIFLUOROMETHYL)-1,3-DISELENETANE

被引：7

作者：

RABE, G ^{[1
]}

KELLER, K ^{[1
]}

ROESKY, HW ^{[1
]}

LAGOW, RJ ^{[1
]}

PAUER, F ^{[1
]}

STALKE, D ^{[1
]}

机构：

[1] UNIV GOTTINGEN,INST ANORGAN CHEM,TAMMANNSTR 4,W-3400 GOTTINGEN,GERMANY

来源：

ZEITSCHRIFT FUR NATURFORSCHUNG SECTION B-A JOURNAL OF CHEMICAL SCIENCES | 1991年 / 46卷 / 02期

关键词：

HEXAFLUOROSELENOACETONE; X-RAY;

D O I：

10.1515/znb-1991-0205

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

The reaction of hexafluoroacetone with triphenylphosphane selenide proceeds with elimination of triphenylphosphate oxide to yield 2,2,4,4-tetrakis(trifluormethyl)-1,3-diselenetane (1). Crystals of 1 that are suitable for X-ray crystal structure analysis have been obtained by recrystallization from hexane.

引用

页码：157 / 160

页数：4

共 50 条

[31] Cone of 1,3-alternate conformers of 1,3-bis(ethoxycarbonylmethoxy)-2,4-dihydroxycalix[4]arene and 1,2,3,4-tetrakis(ethoxycarbonylmethoxy)calix[4]arene
Genorio, B
Kobe, J
Giester, G
Leban, I
ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 2003, 59 : O221 - O224
[32] 2,2,4,4-Tetrathio substituted 1,3-dithietanes
Weber, Wolfgang
Chirowodza, Helen
Pasch, Harald
TETRAHEDRON, 2013, 69 (08) : 2017 - 2021
[33] Reaction of {tris[2-(dimethylamino)phenyl]germyl}lithium with elemental selenium: Formation of 2,2,4,4-tetrakis[2-(dimethylamino)phenyl]-1,3,2,4-diselenadigermetane
Kawachi, A
Tanaka, Y
Tamao, K
CHEMISTRY LETTERS, 1999, (01) : 21 - 22
[34] CRYSTAL-STRUCTURE OF 2,2,4,4-TETRAMETHYLCYCLOBUTANE-1,3-DIONE
RICHE, C
COMPTES RENDUS HEBDOMADAIRES DES SEANCES DE L ACADEMIE DES SCIENCES SERIE C, 1972, 275 (10): : 543 - &
[35] Partial and Complete Replacement of the Phenyl Group(s) of 1,1,3,3-Tetraphenyl-2,2,4,4-tetrakis(trimethylsilyl)cyclotetrasilane by Chlorine Atom(s)
Ishida, Shintaro
Ishii, Yosuke
Fukasawa, Tetsuya
Kyushin, Soichiro
CHEMISTRY-A EUROPEAN JOURNAL, 2023, 29 (70)
[36] CRYSTAL-STRUCTURE OF 1,3-BISDIPHENYLCHLOROSILYL-1,3-DIAZA-2,2,4,4-TETRAPHENYLCYCLODISILAZANE
GURKOVA, SN
GUSEV, AI
ALEKSEEV, NV
VAREZHKIN, YM
MORGUNOVA, MM
ZHINKIN, DY
JOURNAL OF STRUCTURAL CHEMISTRY, 1978, 19 (01) : 164 - 166
[37] CRYSTAL-STRUCTURE OF 2,2,4,4-TETRAMETHYL-1,3-CYCLOBUTANEDITHIONE
SHIRRELL, CD
WILLIAMS, DE
ACTA CRYSTALLOGRAPHICA SECTION B-STRUCTURAL SCIENCE, 1973, B 29 (AUG15): : 1648 - 1653
[38] 1,2,3,4-TETRAKIS(METHOXYCARBONYL)CYCLOBUTADIENE!-TETRACARBONYLMOLYBDENUM
SCHARF, HD
STAHLKE, KR
ANGEWANDTE CHEMIE-INTERNATIONAL EDITION, 1970, 9 (10) : 810 - &
[39] POLYCARBONATES FROM THE 2,2,4,4-TETRAMETHYLCYCLOBUTANE-1,3-DIOLS .1. PREPARATION AND STRUCTURE
GAWLAK, M
ROSE, JB
POLYMER, 1963, 4 (04) : 515 - 524
[40] Synthesis, characterization, and reactivity of [LiC(SiMe2H)3]•2THF:: Formation of 1,1,3,3-tetramethyl-2,2,4,4-tetrakis(dimethylsilyl)-1,3-disilacyclobutane, [Me2SiC(SiMe2H)2]2
Hawrelak, EJ
Ladipo, FT
Sata, D
Braddock-Wilking, J
ORGANOMETALLICS, 1999, 18 (09) : 1804 - 1807

← 1 2 3 4 5 →