QUANTITATIVE-ANALYSIS IN MAS NMR OF QUADRUPOLAR NUCLEI

被引：19
|
作者：
TAULELLE, F [1 ]
BESSADA, C [1 ]
MASSIOT, D [1 ]
机构：
[1] CTR RECH PHYS NAUTES TEMP,CNRS,F-45071 ORLEANS 02,FRANCE
来源：
JOURNAL DE CHIMIE PHYSIQUE ET DE PHYSICO-CHIMIE BIOLOGIQUE | 1992年 / 89卷 / 02期
关键词：
D O I：
10.1051/jcp/1992890379
中图分类号：
Q5 [生物化学]; Q7 [分子生物学];
学科分类号：
071010 ; 081704 ;
摘要：
The aim of this contribution is to give some indications on how to acquire an NMR spectrum of a quadrupolar nucleus in MAS conditions in order to perform a quantitative treatment of the data. In MAS conditions, recently, a way to access to the amount of magnetization contained in "the centerband" has been presented. In this paper, it is a experimental protocol which is proposed to get the NMR signal of quadrupolar nuclei in MAS conditions, and processing it, in a way that will allow an accurate quantification of sites populations.
引用
收藏
页码：379 / 385
页数：7
相关论文
共 50 条
  • [41] Two-Dimensional Multiple-Quantum MAS NMR of Quadrupolar Nuclei. Acquisition of the Whole Echo
    Physical Chemistry Laboratory, University of Oxford, South Parks Road, Oxford OX1 3QZ, United Kingdom
    J. Magn. Reson., 1 (279-285):
  • [42] Second-order cross-term interactions in high-resolution MAS NMR of quadrupolar nuclei
    Ashbrook, Sharon E.
    McManus, Jamie
    Thrippleton, Michael J.
    Wimperis, Stephen
    PROGRESS IN NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY, 2009, 55 (02) : 160 - 181
  • [43] Two-dimensional multiple-quantum MAS NMR of quadrupolar nuclei. Acquisition of the whole echo
    Brown, SP
    Wimperis, S
    JOURNAL OF MAGNETIC RESONANCE, 1997, 124 (01) : 279 - 285
  • [44] Two-dimensional satellite-transition MAS NMR of quadrupolar nuclei: shifted echoes, high-spin nuclei and resolution
    Pike, KJ
    Ashbrook, SE
    Wimperis, S
    CHEMICAL PHYSICS LETTERS, 2001, 345 (5-6) : 400 - 408
  • [45] A way of visualizing NMR experiments on quadrupolar nuclei
    Philp, DJ
    Kuchel, PW
    CONCEPTS IN MAGNETIC RESONANCE PART A, 2005, 25A (01) : 40 - 52
  • [46] QUANTITATIVE-ANALYSIS OF THE OCULOMOTOR NUCLEI IN THE MUTANT MICROPHTHALMIC RAT
    TANAKA, K
    OTANI, K
    SUGITA, S
    EXPERIMENTAL NEUROLOGY, 1987, 95 (02) : 472 - 481
  • [47] Spin Squeezing in a Quadrupolar Nuclei NMR System
    Auccaise, R.
    Araujo-Ferreira, A. G.
    Sarthour, R. S.
    Oliveira, I. S.
    Bonagamba, T. J.
    Roditi, I.
    PHYSICAL REVIEW LETTERS, 2015, 114 (04)
  • [48] A System for NMR Stark Spectroscopy of Quadrupolar Nuclei
    Tarasek, Matthew R.
    Kempf, James G.
    JOURNAL OF PHYSICAL CHEMISTRY A, 2010, 114 (18): : 5743 - 5751
  • [49] New NMR techniques for quadrupolar nuclei - Preface
    Anderson, MW
    Duer, MJ
    SOLID STATE NUCLEAR MAGNETIC RESONANCE, 1999, 15 (03) : V - V
  • [50] Correlation NMR spectroscopy involving quadrupolar nuclei
    Amoureux, J. P.
    Trebosc, J.
    Delevoye, L.
    Lafon, O.
    Hu, B.
    Wang, Q.
    SOLID STATE NUCLEAR MAGNETIC RESONANCE, 2009, 35 (01) : 12 - 18
12345