QUANTITATIVE-ANALYSIS IN MAS NMR OF QUADRUPOLAR NUCLEI

被引：19

作者：

TAULELLE, F ^{[1
]}

BESSADA, C ^{[1
]}

MASSIOT, D ^{[1
]}

机构：

[1] CTR RECH PHYS NAUTES TEMP,CNRS,F-45071 ORLEANS 02,FRANCE

来源：

JOURNAL DE CHIMIE PHYSIQUE ET DE PHYSICO-CHIMIE BIOLOGIQUE | 1992年 / 89卷 / 02期

关键词：

D O I：

10.1051/jcp/1992890379

中图分类号：

Q5 [生物化学]; Q7 [分子生物学];

学科分类号：

071010 ; 081704 ;

摘要：

The aim of this contribution is to give some indications on how to acquire an NMR spectrum of a quadrupolar nucleus in MAS conditions in order to perform a quantitative treatment of the data. In MAS conditions, recently, a way to access to the amount of magnetization contained in "the centerband" has been presented. In this paper, it is a experimental protocol which is proposed to get the NMR signal of quadrupolar nuclei in MAS conditions, and processing it, in a way that will allow an accurate quantification of sites populations.

引用

页码：379 / 385

页数：7

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