A CONVENIENT SYNTHESIS OF VINYL SULFIDES

被引：21

作者：

KATRITZKY, AR ^{[1
]}

AFRIDI, AS ^{[1
]}

KUZMIERKIEWICZ, W ^{[1
]}

机构：

[1] UNIV FLORIDA,CTR HETEROCYCL CPDS,GAINESVILLE,FL 32611

来源：

HELVETICA CHIMICA ACTA | 1991年 / 74卷 / 08期

基金：

俄罗斯科学基金会; 美国国家科学基金会; 美国国家卫生研究院;

关键词：

D O I：

10.1002/hlca.19910740830

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

tert-Alkyl sulfides, with an alpha-(1H-benzotriazol-1-yl) group 6 and 13, are readily prepared from N-[(arylthio)methyl]-1H-benzotriazoles 3 and N-(11), respectively, by reaction with BuLi and then with the appropriate electrophile. The tert-alkyl sulfides 6 and 13 are smoothly converted by BF3.OEt2 into vinyl sulfides 5, 7 or 12, respectively, in satisfactory yields.

引用

页码：1931 / 1935

页数：5

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