AN ISOTOPE-DILUTION HIGH-RESOLUTION GAS-CHROMATOGRAPHIC HIGH-RESOLUTION MASS-SPECTROMETRIC METHOD FOR THE DETERMINATION OF COPLANAR POLYCHLORINATED-BIPHENYLS - APPLICATION TO FISH AND MARINE MAMMALS

被引：61

作者：

KUEHL, DW ^{[1
]}

BUTTERWORTH, BC ^{[1
]}

LIBAL, J ^{[1
]}

MARQUIS, P ^{[1
]}

机构：

[1] ASCI CORP,DULUTH,MN 55804

来源：

CHEMOSPHERE | 1991年 / 22卷 / 9-10期

关键词：

D O I：

10.1016/0045-6535(91)90242-6

中图分类号：

X [环境科学、安全科学];

学科分类号：

08 ; 0830 ;

摘要：

Analytical procedures and a quality assurance plan have been developed for the determination of coplanar PCBs in biological tissue at a target level of quantification of 5 pg/g. The methodology is based upon isotope dilution HRGC/HRMS and is analogous to rigorous protocols developed for PCDD/PCDFs. Results from the determination of coplanar PCBs in fish and marine mammals are presented.

引用

页码：849 / 858

页数：10

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