PREPARATION AND CHARACTERIZATION OF TIPS FOR SCANNING TUNNELING MICROSCOPY OF BIOLOGICAL SPECIMENS

被引:12
|
作者
HACKER, B [1 ]
HILLEBRAND, A [1 ]
HARTMANN, T [1 ]
GUCKENBERGER, R [1 ]
机构
[1] MAX PLANCK INST BIOCHEM,W-8033 MARTINSRIED,GERMANY
关键词
D O I
10.1016/0304-3991(92)90475-Y
中图分类号
TH742 [显微镜];
学科分类号
摘要
For scanning tunneling microscopy of biological samples a thin, sharp tip is necessary to resolve the highly corrugated structures of biomacromolecules. By DC etching of tungsten wire in NaOH we obtain tip radii of 5 nm or less in more than 50% of all cases. For tunneling in fluids these tips are insulated by a wax-coating to minimize faradaic currents. Resulting leakage currents are in the range of 5 to 50 pA.
引用
收藏
页码:1514 / 1518
页数:5
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