MINUTE SYNTHESIS OF ELECTROPHILIC ALKENES UNDER MICROWAVE IRRADIATION

被引:2
|
作者
ABDALLAHELAYOUBI, S [1 ]
TEXIERBOULLET, F [1 ]
HAMELIN, J [1 ]
机构
[1] UNIV RENNES 1,CNRS,PHYSICOCHIM STRUCT GRP 3,CAMPUS BEAULIEU,F-35042 RENNES,FRANCE
来源
SYNTHESIS-STUTTGART | 1994年 / 03期
关键词
D O I
暂无
中图分类号
O62 [有机化学];
学科分类号
070303 ; 081704 ;
摘要
Condensation of carbonyl derivatives 2 with active methylene compounds 1 is efficiently achieved, within 3 to 15 minutes under microwave irradiation by a solvent free reaction in the presence of carefully adjusted amounts of piperidine leading to Knoevenagel products 3 in good to excellent yields.
引用
收藏
页码:258 / 260
页数:3
相关论文
共 50 条
  • [41] Synthesis of Nanoparticulate Tungsten Carbide Under Microwave Irradiation
    Essaki, Kenji
    Rees, Eric J.
    Burstein, Gordon T.
    JOURNAL OF THE AMERICAN CERAMIC SOCIETY, 2010, 93 (03) : 692 - 695
  • [42] Synthesis of nanosized carbonated hydroxyapatite under microwave irradiation
    Ran, Xu
    Chen, Jiyong
    Ran, Junguo
    Gou, Li
    Zhang, Xindong
    BIOCERAMICS, VOL 19, PTS 1 AND 2, 2007, 330-332 : 303 - +
  • [43] Simultaneous Synthesis of Pyrazolopyridines and Pyrazolopyrimidinones Under Microwave Irradiation
    Zhang, Li-Jun
    Shi, Da-Xin
    Li, Jia-Rong
    SYNTHETIC COMMUNICATIONS, 2009, 39 (22) : 4010 - 4018
  • [44] Efficient classical synthesis of aminoazines under microwave irradiation
    Mohammadzadeh, Abbas
    Vahdat, Seyed Mohammad
    Derafshian, Esmaiel
    Akhoondi, Somaieh
    IRANIAN CHEMICAL COMMUNICATION, 2014, 2 (02) : 157 - 163
  • [45] Highly Selective Synthesis of Chlorophenols under Microwave Irradiation
    Xiong, Yawen
    Duan, Hongdong
    Meng, Xia
    Ding, Zhaoyun
    Feng, Weichun
    JOURNAL OF CHEMISTRY, 2016, 2016
  • [46] Synthesis of Heterocyclic Aromatic Sulfides under Microwave Irradiation
    Zhang, Bianxiang
    Yang, Lihua
    Shi, Ruixue
    Kang, Yongqiang
    CHINESE JOURNAL OF ORGANIC CHEMISTRY, 2016, 36 (02) : 352 - 357
  • [47] Rapid Synthesis of Alkyloxy Porphyrins Under Microwave Irradiation
    Ren, Qing-Gang
    Fang, Yan-Xiong
    Ji, Hong-Bing
    Wei, Xing-Chuan
    Deng, Yun-Quan
    Zhang, Kun
    SYNTHETIC COMMUNICATIONS, 2009, 39 (01) : 20 - 28
  • [48] Synthesis of triazones in aqueous media under microwave irradiation
    Balalaie, S
    Shokrollahi, A
    INDIAN JOURNAL OF CHEMISTRY SECTION B-ORGANIC CHEMISTRY INCLUDING MEDICINAL CHEMISTRY, 2001, 40 (07): : 612 - 613
  • [49] Synthesis of ranitidine under microwave irradiation in solventless system
    Heravi, MM
    Motamedi, R
    INDIAN JOURNAL OF HETEROCYCLIC CHEMISTRY, 2004, 14 (02) : 171 - 172
  • [50] A convenient procedure for the synthesis of phthalimides under microwave irradiation
    Mogilaiah, K
    Reddy, GR
    INDIAN JOURNAL OF CHEMISTRY SECTION B-ORGANIC CHEMISTRY INCLUDING MEDICINAL CHEMISTRY, 2004, 43 (04): : 882 - 884